Technology Process of C20H29NO4
There total 5 articles about C20H29NO4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C20H27NO5;
With
lithium triethylborohydride;
In
tetrahydrofuran;
at -78 ℃;
With
dihydrogen peroxide;
In
tetrahydrofuran; water;
at 0 ℃;
With
triethylsilane; boron trifluoride diethyl etherate;
In
dichloromethane;
at -78 ℃;
DOI:10.1021/jm201533b
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: dmap / acetonitrile / 48.58 h / 0 - 20 °C
2.1: lithium hexamethyldisilazane / tetrahydrofuran / -78 °C / Inert atmosphere
2.2: -78 °C / Inert atmosphere
3.1: lithium triethylborohydride / tetrahydrofuran / -78 °C
3.2: 0 °C
3.3: -78 °C
With
dmap; lithium triethylborohydride; lithium hexamethyldisilazane;
In
tetrahydrofuran; acetonitrile;
DOI:10.1021/jm201533b
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: perchloric acid / water / 18 h / 20 °C
2.1: dmap / acetonitrile / 48.58 h / 0 - 20 °C
3.1: lithium hexamethyldisilazane / tetrahydrofuran / -78 °C / Inert atmosphere
3.2: -78 °C / Inert atmosphere
4.1: lithium triethylborohydride / tetrahydrofuran / -78 °C
4.2: 0 °C
4.3: -78 °C
With
dmap; perchloric acid; lithium triethylborohydride; lithium hexamethyldisilazane;
In
tetrahydrofuran; water; acetonitrile;
DOI:10.1021/jm201533b