Technology Process of C8H15NO3
There total 3 articles about C8H15NO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydrogencarbonate / 18 h
2: sodium azide / N,N-dimethyl-formamide / 8 h / 60 °C
3: palladium on activated charcoal; hydrogen / methanol; acetic acid / 18 h / 20 °C / 760.05 Torr
With
sodium azide; palladium on activated charcoal; hydrogen; sodium hydrogencarbonate;
In
methanol; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.09.114
- Guidance literature:
-
Multi-step reaction with 4 steps
1: trimethylsilyl bromide; N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide
2: sodium hydrogencarbonate / 18 h
3: sodium azide / N,N-dimethyl-formamide / 8 h / 60 °C
4: palladium on activated charcoal; hydrogen / methanol; acetic acid / 18 h / 20 °C / 760.05 Torr
With
sodium azide; trimethylsilyl bromide; palladium on activated charcoal; hydrogen; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine;
In
methanol; acetic acid; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.09.114
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium azide / N,N-dimethyl-formamide / 8 h / 60 °C
2: palladium on activated charcoal; hydrogen / methanol; acetic acid / 18 h / 20 °C / 760.05 Torr
With
sodium azide; palladium on activated charcoal; hydrogen;
In
methanol; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.09.114
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