CuCl(N-[(5-methylimidazol-4-yl)methylidene]-DL-phenylalanine^(1-))

Base Information

• Chemical Name: CuCl(N-[(5-methylimidazol-4-yl)methylidene]-DL-phenylalanine^(1-))
• CAS No.: 909783-76-2
• Molecular Formula: C₁₄H₁₄ClCuN₃O₂
• Molecular Weight: 355.283
• Mol file: 909783-76-2.mol

Synonyms:

Chemical Property of CuCl(N-[(5-methylimidazol-4-yl)methylidene]-DL-phenylalanine^(1-))

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of CuCl(N-[(5-methylimidazol-4-yl)methylidene]-DL-phenylalanine^(1-))

There total 1 articles about CuCl(N-[(5-methylimidazol-4-yl)methylidene]-DL-phenylalanine^(1-)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

N-[(5-methylimidazol-4-yl)methylidene]-DL-phenylalanine (1164117-94-5) + copper(II) choride dihydrate → [CuCl(C3H2N2(CH3)CHNCH(CH2C6H5)CO2)] (909783-76-2,909706-13-4)

Guidance literature:

In methanol; mixt. was warmed and stirred for 30 min; mixt. was then filtered, filtrate was allowed to stand for several days,during which time crystals pptd., ppt. was filtered, washed with MeOH, dried; elem. anal.;

DOI:10.1246/bcsj.82.458

Reference yield:

CuCl(N-[(5-methylimidazol-4-yl)methylidene]-DL-phenylalanine(1-)) (909783-76-2,909706-13-4) → (Cu(N-[(5-methylimidazol-4-yl)methylidene]-DL-phenylalanine(1-))(H2O))4

Guidance literature:

With NaOH; In water; to Cu-compd. in H2O added aq. 0.1 M NaOH, stirred for 30 min at room temp.; filtered, filtrate stored for several days, filtered, elem. anal.;

DOI:10.1016/j.poly.2011.11.024

upstream raw materials:

N-[(5-methylimidazol-4-yl)methylidene]-DL-phenylalanine

Refernces