(R,R,R,R,R,R)-α-benzyl-ω-(tert-butoxy)hexakis

Base Information

Chemical Name:(R,R,R,R,R,R)-α-benzyl-ω-(tert-butoxy)hexakis
CAS No.:220095-54-5
Molecular Formula:C₃₅H₅₂O₁₃
Molecular Weight:680.79
Hs Code.:

(R,R,R,R,R,R)-α-benzyl-ω-(tert-butoxy)hexakis<oxy(1-methyl-3-oxopropane-1,3-diyl)>

Synonyms:

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Chemical Property of (R,R,R,R,R,R)-α-benzyl-ω-(tert-butoxy)hexakis

Chemical Property:

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Technology Process of (R,R,R,R,R,R)-α-benzyl-ω-(tert-butoxy)hexakis

There total 15 articles about (R,R,R,R,R,R)-α-benzyl-ω-(tert-butoxy)hexakis which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 116761-27-4
(3R)-3-<<(3'R)-3'-(benzyloxy)butanoyl>oxy>butanoic acid tert-butyl ester

: 220095-54-5
(R,R,R,R,R,R)-α-benzyl-ω-(tert-butoxy)hexakis

Guidance literature:: Multi-step reaction with 5 steps

1: 93 percent / H₂ / Pd/C / ethanol; acetic acid / 5 h / Ambient temperature

2: pyridine / CH₂Cl₂ / -78 °C / to RT

3: 98 percent / CF₃COOH / CH₂Cl₂ / 5 h

4: (COCl)2 / CH₂Cl₂; dimethylformamide / Ambient temperature

5: pyridine / CH₂Cl₂ / -78 °C / to RT

With pyridine; oxalyl dichloride; hydrogen; trifluoroacetic acid; palladium on activated charcoal; In ethanol; dichloromethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1002/(SICI)1522-2675(19981216)81:12<2430::AID-HLCA2430>3.0.CO;2-W

Reference yield:

: 110171-06-7
tert-butyl (R)-3-hydroxybutanoate

: 220095-54-5
(R,R,R,R,R,R)-α-benzyl-ω-(tert-butoxy)hexakis

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / CH₂Cl₂ / -78 °C / to RT

2: 93 percent / H₂ / Pd/C / ethanol; acetic acid / 5 h / Ambient temperature

3: pyridine / CH₂Cl₂ / -78 °C / to RT

With pyridine; hydrogen; palladium on activated charcoal; In ethanol; dichloromethane; acetic acid;
DOI:10.1002/(SICI)1522-2675(19981216)81:12<2430::AID-HLCA2430>3.0.CO;2-W

Reference yield:

: 116761-25-2
(R)-3-(benzyloxy)butanoic acid-(tert-butyl)ester

: 220095-54-5
(R,R,R,R,R,R)-α-benzyl-ω-(tert-butoxy)hexakis

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / H₂ / Pd/C / ethanol; acetic acid / Ambient temperature

2: pyridine / CH₂Cl₂ / -78 °C / to RT

3: 93 percent / H₂ / Pd/C / ethanol; acetic acid / 5 h / Ambient temperature

4: pyridine / CH₂Cl₂ / -78 °C / to RT

With pyridine; hydrogen; palladium on activated charcoal; In ethanol; dichloromethane; acetic acid;
DOI:10.1002/(SICI)1522-2675(19981216)81:12<2430::AID-HLCA2430>3.0.CO;2-W