Technology Process of C19H17N5OS
There total 6 articles about C19H17N5OS which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
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Multi-step reaction with 4 steps
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide
2: potassium permanganate; water; sodium hydrogencarbonate; magnesium sulfate / acetone
3: water; sodium carbonate / 1,4-dioxane; ethanol
4: tris-(dibenzylideneacetone)dipalladium(0); sodium carbonate; triphenylphosphine / water; N,N-dimethyl-formamide
With
bis-triphenylphosphine-palladium(II) chloride; potassium permanganate; tris-(dibenzylideneacetone)dipalladium(0); copper(l) iodide; water; sodium hydrogencarbonate; sodium carbonate; magnesium sulfate; triethylamine; triphenylphosphine;
In
1,4-dioxane; ethanol; water; N,N-dimethyl-formamide; acetone;
1: Sonogashira coupling;
DOI:10.1016/j.bmcl.2011.07.057
- Guidance literature:
-
Multi-step reaction with 2 steps
1: water; sodium carbonate / 1,4-dioxane; ethanol
2: tris-(dibenzylideneacetone)dipalladium(0); sodium carbonate; triphenylphosphine / water; N,N-dimethyl-formamide
With
tris-(dibenzylideneacetone)dipalladium(0); water; sodium carbonate; triphenylphosphine;
In
1,4-dioxane; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.07.057
- Guidance literature:
-
Multi-step reaction with 4 steps
1: n-butyllithium / toluene
2: potassium permanganate; water; sodium hydrogencarbonate; magnesium sulfate / acetone
3: water; sodium carbonate / 1,4-dioxane; ethanol
4: tris-(dibenzylideneacetone)dipalladium(0); sodium carbonate; triphenylphosphine / water; N,N-dimethyl-formamide
With
potassium permanganate; tris-(dibenzylideneacetone)dipalladium(0); n-butyllithium; water; sodium hydrogencarbonate; sodium carbonate; magnesium sulfate; triphenylphosphine;
In
1,4-dioxane; ethanol; water; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1016/j.bmcl.2011.07.057