2-Tetradecyl-hexadecanoic acid (2R,3R,4R,5S,6R)-2-benzyloxy-6-benzyloxymethoxymethyl-5-(diphenoxy-phosphoryloxy)-3-(3-hydroxy-tetradecanoylamino)-tetrahydro-pyran-4-yl ester

Base Information

Chemical Name:2-Tetradecyl-hexadecanoic acid (2R,3R,4R,5S,6R)-2-benzyloxy-6-benzyloxymethoxymethyl-5-(diphenoxy-phosphoryloxy)-3-(3-hydroxy-tetradecanoylamino)-tetrahydro-pyran-4-yl ester
CAS No.:124710-53-8
Molecular Formula:C₇₇H₁₂₀NO₁₂P
Molecular Weight:1282.77
Hs Code.:

2-Tetradecyl-hexadecanoic acid (2R,3R,4R,5S,6R)-2-benzyloxy-6-benzyloxymethoxymethyl-5-(diphenoxy-phosphoryloxy)-3-(3-hydroxy-tetradecanoylamino)-tetrahydro-pyran-4-yl ester

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Chemical Property of 2-Tetradecyl-hexadecanoic acid (2R,3R,4R,5S,6R)-2-benzyloxy-6-benzyloxymethoxymethyl-5-(diphenoxy-phosphoryloxy)-3-(3-hydroxy-tetradecanoylamino)-tetrahydro-pyran-4-yl ester

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Technology Process of 2-Tetradecyl-hexadecanoic acid (2R,3R,4R,5S,6R)-2-benzyloxy-6-benzyloxymethoxymethyl-5-(diphenoxy-phosphoryloxy)-3-(3-hydroxy-tetradecanoylamino)-tetrahydro-pyran-4-yl ester

There total 9 articles about 2-Tetradecyl-hexadecanoic acid (2R,3R,4R,5S,6R)-2-benzyloxy-6-benzyloxymethoxymethyl-5-(diphenoxy-phosphoryloxy)-3-(3-hydroxy-tetradecanoylamino)-tetrahydro-pyran-4-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1961-72-4,3422-31-9
3-hydroxytetradecanoic acid

: 124710-44-7
Benzyl 2-amino-6-O-benzyloxymethyl-2-deoxy-4-O-(diphenoxyphosphinyl)-3-O-(2-tetradecylhexadecanoyl)-β-D-glucopyranoside

: 124710-53-8,124710-71-0
2-Tetradecyl-hexadecanoic acid (2R,3R,4R,5S,6R)-2-benzyloxy-6-benzyloxymethoxymethyl-5-(diphenoxy-phosphoryloxy)-3-(3-hydroxy-tetradecanoylamino)-tetrahydro-pyran-4-yl ester

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; Ambient temperature;
DOI:10.1016/0008-6215(91)80013-D

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: 124710-53-8,124710-71-0
2-Tetradecyl-hexadecanoic acid (2R,3R,4R,5S,6R)-2-benzyloxy-6-benzyloxymethoxymethyl-5-(diphenoxy-phosphoryloxy)-3-(3-hydroxy-tetradecanoylamino)-tetrahydro-pyran-4-yl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 52 percent / 1,1,3,3-tetramethylurea / CH₂Cl₂ / Ambient temperature

2: 4-dimethylaminopyridine, pyridine / CH₂Cl₂ / Ambient temperature

3: 1.8 g / zinc dust, acetic acid / 3 h / 60 °C

4: 80 percent / 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride / CH₂Cl₂ / Ambient temperature

With pyridine; dmap; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; tetramethylurea; zinc; In dichloromethane;
DOI:10.1016/0008-6215(91)80013-D

Reference yield:

: 66880-77-1
2-tetradecylhexadecanoic acid

: 124710-53-8,124710-71-0
2-Tetradecyl-hexadecanoic acid (2R,3R,4R,5S,6R)-2-benzyloxy-6-benzyloxymethoxymethyl-5-(diphenoxy-phosphoryloxy)-3-(3-hydroxy-tetradecanoylamino)-tetrahydro-pyran-4-yl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 97 percent / 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride, 4-dimethylaminopyridine / 1,2-dichloro-ethane / Ambient temperature

2: 3.5 g / 80percent aq. acetic acid / 3 h / 50 °C

3: 52 percent / 1,1,3,3-tetramethylurea / CH₂Cl₂ / Ambient temperature

4: 4-dimethylaminopyridine, pyridine / CH₂Cl₂ / Ambient temperature

5: 1.8 g / zinc dust, acetic acid / 3 h / 60 °C

6: 80 percent / 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride / CH₂Cl₂ / Ambient temperature

With pyridine; dmap; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; tetramethylurea; zinc; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1016/0008-6215(91)80013-D