5-[4-((4,6-(bis)piperidyl)-1,3,5-triazinyl)aminophenyl]-10,20-bis(mesityl)-15-(4-N-methylpyridinium)porphyrin

Base Information

• Chemical Name: 5-[4-((4,6-(bis)piperidyl)-1,3,5-triazinyl)aminophenyl]-10,20-bis(mesityl)-15-(4-N-methylpyridinium)porphyrin
• CAS No.: 1264173-54-7
• Molecular Formula: C₆₃H₆₄N₁₁*HO
• Molecular Weight: 992.282
• Mol file: 1264173-54-7.mol

Synonyms:

Chemical Property of 5-[4-((4,6-(bis)piperidyl)-1,3,5-triazinyl)aminophenyl]-10,20-bis(mesityl)-15-(4-N-methylpyridinium)porphyrin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-[4-((4,6-(bis)piperidyl)-1,3,5-triazinyl)aminophenyl]-10,20-bis(mesityl)-15-(4-N-methylpyridinium)porphyrin

There total 5 articles about 5-[4-((4,6-(bis)piperidyl)-1,3,5-triazinyl)aminophenyl]-10,20-bis(mesityl)-15-(4-N-methylpyridinium)porphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-(mesityl)dipyrromethane (159152-14-4) → 5-[4-((4,6-(bis)piperidyl)-1,3,5-triazinyl)aminophenyl]-10,20-bis(mesityl)-15-(4-N-methylpyridinium)porphyrin (1264173-54-7)

Guidance literature:

Multi-step reaction with 5 steps

1.1: trifluoroacetic acid / dichloromethane / Inert atmosphere

1.2: 1.5 h / 20 °C / Inert atmosphere

2.1: N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

3.1: hydrogenchloride; acetic acid; tin(ll) chloride / chloroform; water / 70 - 80 °C

4.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0 - 20 °C

5.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 24 h / Reflux

With hydrogenchloride; acetic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; tin(ll) chloride; In tetrahydrofuran; dichloromethane; chloroform; water; N,N-dimethyl-formamide;

DOI:10.1142/S1088424610002719

Reference yield:

C50H43N6O2(1+)*I(1-) → 5-[4-((4,6-(bis)piperidyl)-1,3,5-triazinyl)aminophenyl]-10,20-bis(mesityl)-15-(4-N-methylpyridinium)porphyrin (1264173-54-7)

Guidance literature:

Multi-step reaction with 3 steps

1: hydrogenchloride; acetic acid; tin(ll) chloride / chloroform; water / 70 - 80 °C

2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0 - 20 °C

3: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 24 h / Reflux

With hydrogenchloride; acetic acid; N-ethyl-N,N-diisopropylamine; tin(ll) chloride; In tetrahydrofuran; chloroform; water;

DOI:10.1142/S1088424610002719

Reference yield:

5-(4-aminophenyl)-10,20-bis(mesityl)-15-(4-N-methylpyridinium)porphyrin (1264173-50-3) → 5-[4-((4,6-(bis)piperidyl)-1,3,5-triazinyl)aminophenyl]-10,20-bis(mesityl)-15-(4-N-methylpyridinium)porphyrin (1264173-54-7)

Guidance literature:

Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0 - 20 °C

2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 24 h / Reflux

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran;

DOI:10.1142/S1088424610002719

upstream raw materials:

piperidine

C₅₃H₄₄Cl₂N₉⁽¹⁺⁾*HO^(1-)

5-(4-aminophenyl)-10,20-bis(mesityl)-15-(4-N-methylpyridinium)porphyrin

4-nitrobenzaldehdye