(1S,2S,3S,4R,5R)-4-Benzyloxy-2-((1S,2S,3R,4S,5R,6S)-3,4,5,6-tetrakis-benzyloxy-3-benzyloxymethyl-2-hydroxy-cyclohexylamino)-6,8-dioxa-bicyclo[3.2.1]octan-3-ol

Base Information

Chemical Name:(1S,2S,3S,4R,5R)-4-Benzyloxy-2-((1S,2S,3R,4S,5R,6S)-3,4,5,6-tetrakis-benzyloxy-3-benzyloxymethyl-2-hydroxy-cyclohexylamino)-6,8-dioxa-bicyclo[3.2.1]octan-3-ol
CAS No.:122901-33-1
Molecular Formula:C₅₅H₅₉NO₁₀
Molecular Weight:894.074
Hs Code.:

(1S,2S,3S,4R,5R)-4-Benzyloxy-2-((1S,2S,3R,4S,5R,6S)-3,4,5,6-tetrakis-benzyloxy-3-benzyloxymethyl-2-hydroxy-cyclohexylamino)-6,8-dioxa-bicyclo[3.2.1]octan-3-ol

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Chemical Property of (1S,2S,3S,4R,5R)-4-Benzyloxy-2-((1S,2S,3R,4S,5R,6S)-3,4,5,6-tetrakis-benzyloxy-3-benzyloxymethyl-2-hydroxy-cyclohexylamino)-6,8-dioxa-bicyclo[3.2.1]octan-3-ol

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Technology Process of (1S,2S,3S,4R,5R)-4-Benzyloxy-2-((1S,2S,3R,4S,5R,6S)-3,4,5,6-tetrakis-benzyloxy-3-benzyloxymethyl-2-hydroxy-cyclohexylamino)-6,8-dioxa-bicyclo[3.2.1]octan-3-ol

There total 1 articles about (1S,2S,3S,4R,5R)-4-Benzyloxy-2-((1S,2S,3R,4S,5R,6S)-3,4,5,6-tetrakis-benzyloxy-3-benzyloxymethyl-2-hydroxy-cyclohexylamino)-6,8-dioxa-bicyclo[3.2.1]octan-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106989-01-9
1L-2-azido-1,4,5,6-tetra-O-benzyl-2-desoxy-4-C-(benzyloxymethyl)-muco-inosit

: 122901-33-1
(1S,2S,3S,4R,5R)-4-Benzyloxy-2-((1S,2S,3R,4S,5R,6S)-3,4,5,6-tetrakis-benzyloxy-3-benzyloxymethyl-2-hydroxy-cyclohexylamino)-6,8-dioxa-bicyclo[3.2.1]octan-3-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / NaBH₄ / 4 percent NiCl₂ / ethanol

2: propan-1-ol / 30 h / 90 °C

With sodium tetrahydroborate; nickel dichloride; In propan-1-ol; ethanol;

Reference yield:

: 122901-33-1
(1S,2S,3S,4R,5R)-4-Benzyloxy-2-((1S,2S,3R,4S,5R,6S)-3,4,5,6-tetrakis-benzyloxy-3-benzyloxymethyl-2-hydroxy-cyclohexylamino)-6,8-dioxa-bicyclo[3.2.1]octan-3-ol

: 122901-38-6
methyl-4-desoxy-4-<1D-(1N,2,4,5/3,6)-(5-C-hydroxymethyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine

2: 89 percent / BF₃-diethyl ether / 4 h / Ambient temperature

3: 157 mg / HBr / CH₂Cl₂ / 1 h / Ambient temperature

4: 53 percent / Ag₂CO₃, AgClO₄ / CH₂Cl₂; toluene / 5 h / -30 °C

5: 1) H₂, 2) pyridine / 1) Pd/C (10percent) / 1) CH₃OH, 1 atm, 24 h

6: 63 percent / 0.1 N CH₃ONa / methanol / 3 h

With pyridine; boron trifluoride diethyl etherate; hydrogen bromide; hydrogen; sodium methylate; silver perchlorate; silver carbonate; palladium on activated charcoal; In methanol; dichloromethane; toluene;

Reference yield:

: 122901-33-1
(1S,2S,3S,4R,5R)-4-Benzyloxy-2-((1S,2S,3R,4S,5R,6S)-3,4,5,6-tetrakis-benzyloxy-3-benzyloxymethyl-2-hydroxy-cyclohexylamino)-6,8-dioxa-bicyclo[3.2.1]octan-3-ol

: 122901-37-5
methyl-4-<1D-(1N,2,4,5/3,6)-(5-C-acetoxymethyl-2,3,4,6-tetra-O-acetyl-2,3,4,5,6-pentahydroxycyclohexyl)amino>-2,3,6-tri-O-acetyl-4-desoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine

2: 89 percent / BF₃-diethyl ether / 4 h / Ambient temperature

3: 157 mg / HBr / CH₂Cl₂ / 1 h / Ambient temperature

4: 53 percent / Ag₂CO₃, AgClO₄ / CH₂Cl₂; toluene / 5 h / -30 °C

5: 1) H₂, 2) pyridine / 1) Pd/C (10percent) / 1) CH₃OH, 1 atm, 24 h

With pyridine; boron trifluoride diethyl etherate; hydrogen bromide; hydrogen; silver perchlorate; silver carbonate; palladium on activated charcoal; In dichloromethane; toluene;