{Ru(CO₂Et)(CO)2(triphos)}PF₆

Base Information

Chemical Name:{Ru(CO₂Et)(CO)2(triphos)}PF₆
CAS No.:121393-27-9
Molecular Formula:C₄₆H₄₄O₄P₃Ru*F₆P
Molecular Weight:999.808
Hs Code.:

{Ru(CO<sub>2</sub>Et)(CO)2(triphos)}PF<sub>6</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {Ru(CO₂Et)(CO)2(triphos)}PF₆

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of {Ru(CO₂Et)(CO)2(triphos)}PF₆

There total 3 articles about {Ru(CO₂Et)(CO)2(triphos)}PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: sodium hexaflorophosphate

: 47876-61-9
{RuCl(CO)2(triphos)}⁽¹⁺⁾

: 121374-01-4
{Ru(CO)3(triphos)}PF₆

: 121393-27-9
{Ru(CO₂Et)(CO)2(triphos)}PF₆

Guidance literature:: With aluminium trichloride; ethanol; carbon monoxide; In dichloromethane; byproducts: AlCl4(1-); mixt. of chloro complex/AlCl3 treated with CO (1 atm, room temp.), stirred 10 min, further AlCl3 and solvent added, stirred (CO) for 20 min, evapd., residue dissolved in EtOH, NaPF6 added; ppt. extd. with CH2Cl2, (residue: tricarbonyl complex, not analytically pure), ext.: ethoxycarbonyl complex recrystd. from EtOH/Et2O; elem. anal.;
DOI:10.1021/om00110a012

Reference yield:

: sodium hexaflorophosphate

: 99299-44-2
{RuBr(CO)2(triphos)}⁽¹⁺⁾

: 121374-01-4
{Ru(CO)3(triphos)}PF₆

: 121393-27-9
{Ru(CO₂Et)(CO)2(triphos)}PF₆

Guidance literature:: With aluminium trichloride; ethanol; carbon monoxide; In dichloromethane; byproducts: AlCl4(1-); mixt. of chloro complex/AlCl3 treated with CO (1 atm, room temp.), stirred 10 min, further AlCl3 and solvent added, stirred (CO) for 20 min, evapd., residue dissolved in EtOH, NaPF6 added; ppt. extd. with CH2Cl2, (residue: tricarbonyl complex, not analytically pure), ext.: ethoxycarbonyl complex recrystd. from EtOH/Et2O; elem. anal.;
DOI:10.1021/om00110a012

Reference yield:

: sodium hexaflorophosphate

: 99299-47-5
{RuI(CO)2(triphos)}⁽¹⁺⁾

: 121374-01-4
{Ru(CO)3(triphos)}PF₆

: 121393-27-9
{Ru(CO₂Et)(CO)2(triphos)}PF₆

Guidance literature:: With aluminium trichloride; ethanol; carbon monoxide; In dichloromethane; byproducts: AlCl4(1-); mixt. of chloro complex/AlCl3 treated with CO (1 atm, room temp.), stirred 10 min, further AlCl3 and solvent added, stirred (CO) for 20 min, evapd., residue dissolved in EtOH, NaPF6 added; ppt. extd. with CH2Cl2, (residue: tricarbonyl complex, not analytically pure), ext.: ethoxy carbonyl complex recrystd. from EtOH/Et2O; elem. anal.;
DOI:10.1021/om00110a012