phenyl p-guanidinophenylpropionate methanesulfonate

Base Information

Chemical Name:phenyl p-guanidinophenylpropionate methanesulfonate
CAS No.:93130-71-3
Molecular Formula:CH₄O₃S*C₁₆H₁₇N₃O₂
Molecular Weight:379.437
Hs Code.:

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Chemical Property of phenyl p-guanidinophenylpropionate methanesulfonate

Chemical Property:

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Technology Process of phenyl p-guanidinophenylpropionate methanesulfonate

There total 5 articles about phenyl p-guanidinophenylpropionate methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 93130-50-8
phenyl p-guanidinocinnamate methanesulfonate

: 93130-71-3
phenyl p-guanidinophenylpropionate methanesulfonate

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; Ambient temperature;
DOI:10.1248/cpb.32.1854

Reference yield:

: 882-06-4
4-nitro-trans-cinnamic acid

: 93130-71-3
phenyl p-guanidinophenylpropionate methanesulfonate

Guidance literature:: Multi-step reaction with 5 steps

1: PCl₅ / ethyl acetate / 3 h / Ambient temperature

2: triethylamine / ethyl acetate / 3 h / Ambient temperature

3: 1) Zn / 1) acetic acid, RT

4: 1) MeOH, 50 deg C; 2) EtOH

5: H₂ / 10 percent Pd-C / methanol / Ambient temperature

With phosphorus pentachloride; hydrogen; triethylamine; zinc; palladium on activated charcoal; In methanol; ethyl acetate;
DOI:10.1248/cpb.32.1854

Reference yield:

: 13546-92-4
phenyl p-nitrocinnamate

: 93130-71-3
phenyl p-guanidinophenylpropionate methanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: 1) Zn / 1) acetic acid, RT

2: 1) MeOH, 50 deg C; 2) EtOH

3: H₂ / 10 percent Pd-C / methanol / Ambient temperature

With hydrogen; zinc; palladium on activated charcoal; In methanol;
DOI:10.1248/cpb.32.1854