C₂HF₃O₂*C₃₃H₄₁N₉O₈

Base Information

Chemical Name:C₂HF₃O₂*C₃₃H₄₁N₉O₈
CAS No.:1389332-12-0
Molecular Formula:C₂HF₃O₂*C₃₃H₄₁N₉O₈
Molecular Weight:805.768
Hs Code.:

C<sub>2</sub>HF<sub>3</sub>O<sub>2</sub>*C<sub>33</sub>H<sub>41</sub>N<sub>9</sub>O<sub>8</sub>

Synonyms:

Suppliers and Price of C₂HF₃O₂*C₃₃H₄₁N₉O₈

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂HF₃O₂*C₃₃H₄₁N₉O₈

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂HF₃O₂*C₃₃H₄₁N₉O₈

There total 12 articles about C₂HF₃O₂*C₃₃H₄₁N₉O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1389332-48-2
C₆₂H₇₅N₉O₁₄S

: 1389332-12-0
C₂HF₃O₂*C₃₃H₄₁N₉O₈

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; water / 20 °C / 750.08 Torr / Inert atmosphere

2: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 1 h / 0 °C / Inert atmosphere

3: methyl-phenyl-thioether; ethane-1,2-dithiol; methoxybenzene / Inert atmosphere

With 1-hydroxy-7-aza-benzotriazole; methyl-phenyl-thioether; palladium 10% on activated carbon; hydrogen; ethane-1,2-dithiol; methoxybenzene; N-ethyl-N,N-diisopropylamine; HATU; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201200457

Reference yield:

: C₂HF₃O₂*C₁₆H₂₁N₅O₅

: 1389332-12-0
C₂HF₃O₂*C₃₃H₄₁N₉O₈

Guidance literature:: Multi-step reaction with 10 steps

1.1: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 5 h / 20 °C / Inert atmosphere

2.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 °C / Inert atmosphere

2.2: 3 h / -40 °C / Inert atmosphere

3.1: trimethylphosphane / tetrahydrofuran; toluene / 6 h / -20 - 20 °C / Inert atmosphere

4.1: lithium hydroxide monohydrate / tetrahydrofuran; water / 1 h / 0 °C / Inert atmosphere

5.1: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

5.2: 0 - 20 °C / Inert atmosphere

6.1: dichloromethane / 2 h / 20 °C / Inert atmosphere

7.1: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

7.2: 0 - 20 °C / Inert atmosphere

8.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; water / 20 °C / 750.08 Torr / Inert atmosphere

9.1: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 1 h / 0 °C / Inert atmosphere

10.1: methyl-phenyl-thioether; ethane-1,2-dithiol; methoxybenzene / Inert atmosphere

With 1-hydroxy-7-aza-benzotriazole; lithium hydroxide monohydrate; methyl-phenyl-thioether; palladium 10% on activated carbon; hydrogen; potassium hexamethylsilazane; ethane-1,2-dithiol; methoxybenzene; N-ethyl-N,N-diisopropylamine; HATU; trimethylphosphane; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol; toluene;
DOI:10.1002/chem.201200457

Reference yield:

: 1389332-02-8
C₂₁H₂₉N₅O₇

: 1389332-12-0
C₂HF₃O₂*C₃₃H₄₁N₉O₈

Guidance literature:: Multi-step reaction with 11 steps

1.1: triethylsilane / dichloromethane / 2 h / 20 °C / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 5 h / 20 °C / Inert atmosphere

3.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 °C / Inert atmosphere

3.2: 3 h / -40 °C / Inert atmosphere

4.1: trimethylphosphane / tetrahydrofuran; toluene / 6 h / -20 - 20 °C / Inert atmosphere

5.1: lithium hydroxide monohydrate / tetrahydrofuran; water / 1 h / 0 °C / Inert atmosphere

6.1: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

6.2: 0 - 20 °C / Inert atmosphere

7.1: dichloromethane / 2 h / 20 °C / Inert atmosphere

8.1: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

8.2: 0 - 20 °C / Inert atmosphere

9.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; water / 20 °C / 750.08 Torr / Inert atmosphere

10.1: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 1 h / 0 °C / Inert atmosphere

11.1: methyl-phenyl-thioether; ethane-1,2-dithiol; methoxybenzene / Inert atmosphere

With triethylsilane; 1-hydroxy-7-aza-benzotriazole; lithium hydroxide monohydrate; methyl-phenyl-thioether; palladium 10% on activated carbon; hydrogen; potassium hexamethylsilazane; ethane-1,2-dithiol; methoxybenzene; N-ethyl-N,N-diisopropylamine; HATU; trimethylphosphane; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol; toluene;
DOI:10.1002/chem.201200457