4-{4-[1-(4-{1-[4-(3-chlorocarbonyl-propoxy)-3,5-dimethyl-phenyl]-1-methyl-ethyl}-phenyl)-1-methyl-ethyl]-2,6-dimethyl-phenoxy}-butyryl chloride

Base Information

Chemical Name:4-{4-[1-(4-{1-[4-(3-chlorocarbonyl-propoxy)-3,5-dimethyl-phenyl]-1-methyl-ethyl}-phenyl)-1-methyl-ethyl]-2,6-dimethyl-phenoxy}-butyryl chloride
CAS No.:871240-20-9
Molecular Formula:C₃₆H₄₄Cl₂O₄
Molecular Weight:611.649
Hs Code.:

4-{4-[1-(4-{1-[4-(3-chlorocarbonyl-propoxy)-3,5-dimethyl-phenyl]-1-methyl-ethyl}-phenyl)-1-methyl-ethyl]-2,6-dimethyl-phenoxy}-butyryl chloride

Synonyms:

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Chemical Property of 4-{4-[1-(4-{1-[4-(3-chlorocarbonyl-propoxy)-3,5-dimethyl-phenyl]-1-methyl-ethyl}-phenyl)-1-methyl-ethyl]-2,6-dimethyl-phenoxy}-butyryl chloride

Chemical Property:

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Technology Process of 4-{4-[1-(4-{1-[4-(3-chlorocarbonyl-propoxy)-3,5-dimethyl-phenyl]-1-methyl-ethyl}-phenyl)-1-methyl-ethyl]-2,6-dimethyl-phenoxy}-butyryl chloride

There total 5 articles about 4-{4-[1-(4-{1-[4-(3-chlorocarbonyl-propoxy)-3,5-dimethyl-phenyl]-1-methyl-ethyl}-phenyl)-1-methyl-ethyl]-2,6-dimethyl-phenoxy}-butyryl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 871240-19-6
4-{4-[1-(4-{1-[4-(3-carboxy-propoxy)-3,5-dimethyl-phenyl]-1-methyl-ethyl}-phenyl)-1-methyl-ethyl]-2,6-dimethyl-phenoxy}-butyric acid

: 871240-20-9
4-{4-[1-(4-{1-[4-(3-chlorocarbonyl-propoxy)-3,5-dimethyl-phenyl]-1-methyl-ethyl}-phenyl)-1-methyl-ethyl]-2,6-dimethyl-phenoxy}-butyryl chloride

Guidance literature:: With thionyl chloride; N,N-dimethyl-formamide; In benzene; for 3h; Heating;
DOI:10.1002/poc.981

Reference yield:

: 871240-18-5
4-{4-[1-(4-{1-[4-(3-ethoxycarbonyl-propoxy)-3,5-dimethyl-phenyl]-1-methyl-ethyl}-phenyl)-1-methyl-ethyl]-2,6-dimethyl-phenoxy}-butyric acid ethyl ester

: 871240-20-9
4-{4-[1-(4-{1-[4-(3-chlorocarbonyl-propoxy)-3,5-dimethyl-phenyl]-1-methyl-ethyl}-phenyl)-1-methyl-ethyl]-2,6-dimethyl-phenoxy}-butyryl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / KOH / ethanol; H₂O / 1 h / Heating

2: 2.10 g / SOCl₂ / DMF / benzene / 3 h / Heating

With potassium hydroxide; thionyl chloride; N,N-dimethyl-formamide; In ethanol; water; benzene;
DOI:10.1002/poc.981

Reference yield:

: 576-26-1,25134-01-4
2.6-dimethylphenol

: 871240-20-9
4-{4-[1-(4-{1-[4-(3-chlorocarbonyl-propoxy)-3,5-dimethyl-phenyl]-1-methyl-ethyl}-phenyl)-1-methyl-ethyl]-2,6-dimethyl-phenoxy}-butyryl chloride

Guidance literature:: Multi-step reaction with 4 steps

1: 73 percent / HCl / 3.5 h / 80 °C

2: 88 percent / K₂CO₃ / acetone / 24 h / Heating

3: 93 percent / KOH / ethanol; H₂O / 1 h / Heating

4: 2.10 g / SOCl₂ / DMF / benzene / 3 h / Heating

With hydrogenchloride; potassium hydroxide; thionyl chloride; potassium carbonate; N,N-dimethyl-formamide; In ethanol; water; acetone; benzene;
DOI:10.1002/poc.981