4-n-hexyloxybenzonitrile oxide

Base Information

• Chemical Name: 4-n-hexyloxybenzonitrile oxide
• CAS No.: 865487-84-9
• Molecular Formula: C₁₃H₁₇NO₂
• Molecular Weight: 219.283
• Mol file: 865487-84-9.mol

Synonyms:

Chemical Property of 4-n-hexyloxybenzonitrile oxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-n-hexyloxybenzonitrile oxide

There total 4 articles about 4-n-hexyloxybenzonitrile oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-n-hexyloxybenzaldehyde oxime (61096-88-6) → 4-n-hexyloxybenzonitrile oxide (865487-84-9)

Guidance literature:

With chloroamine-T; In ethanol;

Reference yield:

1-bromo-hexane (111-25-1) → 4-n-hexyloxybenzonitrile oxide (865487-84-9)

Guidance literature:

Multi-step reaction with 3 steps

1: KOH; phase transfer / tetrahydrofuran

2: H₂N-OH*HCl; CH₃COONa / ethanol

3: chloramine-T / ethanol

With potassium hydroxide; hydroxylamine hydrochloride; sodium acetate; chloroamine-T; In tetrahydrofuran; ethanol;

Reference yield:

4-(hexyloxy)benzaldehyde (5736-94-7) → 4-n-hexyloxybenzonitrile oxide (865487-84-9)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂N-OH*HCl; CH₃COONa / ethanol

2: chloramine-T / ethanol

With hydroxylamine hydrochloride; sodium acetate; chloroamine-T; In ethanol;

upstream raw materials:

4-n-hexyloxybenzaldehyde oxime

1-bromo-hexane

4-(hexyloxy)benzaldehyde

4-hydroxy-benzaldehyde

Refernces