2-PROPYNYL 5H-[1,2,4]TRIAZINO[5,6-B]INDOL-3-YL SULFIDE

Base Information

• Chemical Name: 2-PROPYNYL 5H-[1,2,4]TRIAZINO[5,6-B]INDOL-3-YL SULFIDE
• CAS No.: 332110-23-3
• Molecular Formula: C₁₂H₈N₄S
• Molecular Weight: 240.288
• Mol file: 332110-23-3.mol

Synonyms:

Chemical Property of 2-PROPYNYL 5H-[1,2,4]TRIAZINO[5,6-B]INDOL-3-YL SULFIDE

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

2-Propynyl 5H-[1,2,4]triazino[5,6-b]indol-3-yl sulfide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-PROPYNYL 5H-[1,2,4]TRIAZINO[5,6-B]INDOL-3-YL SULFIDE

There total 2 articles about 2-PROPYNYL 5H-[1,2,4]TRIAZINO[5,6-B]INDOL-3-YL SULFIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

3-mercapto-5H-1,2,4-triazino[5,6-b]indole (28668-95-3) + propargyl bromide (106-96-7) → 3-(prop-2-yn-1-ylsulfanyl)-5H-[1,2,4]triazino[5,6-b]indole (332110-23-3)

Guidance literature:

With water; sodium hydroxide; In dimethyl sulfoxide; at 20 ℃; for 1.5h;

DOI:10.1007/s10593-010-0421-5

Reference yield:

2,5-dihydro-3H-1,2,4-triazino[5,6-b]indole-3-thione (28668-95-3) + propargyl bromide (106-96-7) → 3-(prop-2-yn-1-ylsulfanyl)-5H-[1,2,4]triazino[5,6-b]indole (332110-23-3)

Guidance literature:

With sodium hydroxide; In water; dimethyl sulfoxide;

DOI:10.1134/S1070428015070209

upstream raw materials:

3-mercapto-5H-1,2,4-triazino[5,6-b]indole

propargyl bromide

2,5-dihydro-3H-1,2,4-triazino[5,6-b]indole-3-thione