Technology Process of C20H30BNO2*ClH
There total 4 articles about C20H30BNO2*ClH which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C20H28BN3O2;
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
Inert atmosphere;
With
hydrogenchloride;
In
methanol;
Inert atmosphere;
DOI:10.1111/cbdd.12091
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium azide; tetrabutylammomium bromide / dichloromethane; water / Inert atmosphere
2.1: n-butyllithium / tetrahydrofuran / -100 °C / Inert atmosphere
2.2: -78 °C / Inert atmosphere
3.1: zinc(II) chloride / tetrahydrofuran / -78 °C / Inert atmosphere
4.1: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere
4.2: Inert atmosphere
With
lithium aluminium tetrahydride; n-butyllithium; sodium azide; tetrabutylammomium bromide; zinc(II) chloride;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.1111/cbdd.12091
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium / tetrahydrofuran / -100 °C / Inert atmosphere
1.2: -78 °C / Inert atmosphere
2.1: zinc(II) chloride / tetrahydrofuran / -78 °C / Inert atmosphere
3.1: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere
3.2: Inert atmosphere
With
lithium aluminium tetrahydride; n-butyllithium; zinc(II) chloride;
In
tetrahydrofuran;
DOI:10.1111/cbdd.12091
