C₆₉H₁₀₀N₁₂O₉Si₂

Base Information

Chemical Name:C₆₉H₁₀₀N₁₂O₉Si₂
CAS No.:1431217-33-2
Molecular Formula:C₆₉H₁₀₀N₁₂O₉Si₂
Molecular Weight:1297.8
Hs Code.:

C<sub>69</sub>H<sub>100</sub>N<sub>12</sub>O<sub>9</sub>Si<sub>2</sub>

Synonyms:

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Chemical Property of C₆₉H₁₀₀N₁₂O₉Si₂

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Technology Process of C₆₉H₁₀₀N₁₂O₉Si₂

There total 12 articles about C₆₉H₁₀₀N₁₂O₉Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (R)-2-{[((9H-fluoren-9-yl)methoxy)carbonyl]amino}-6-azidohexanoic acid

: 1431217-33-2
C₆₉H₁₀₀N₁₂O₉Si₂

Guidance literature:: Multi-step reaction with 3 steps

1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h

2: trifluoroacetic acid / dichloromethane / 1 h

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h

With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1039/c3cc40628h

Reference yield:

: 1431217-29-6
C₂₈H₃₅N₅O₅

: 1431217-33-2
C₆₉H₁₀₀N₁₂O₉Si₂

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 1 h

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1039/c3cc40628h

Reference yield:

: 792892-61-6
(R)-4'-hydroxy-3',5'-diiodophenylglycine

: 1431217-33-2
C₆₉H₁₀₀N₁₂O₉Si₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / water; 1,4-dioxane

1.2: pH 2 - 3

2.1: sodium hydroxide / dichloromethane; water / 3 h / 0 - 20 °C

2.2: pH 2 - 3

3.1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 h / 20 °C / Inert atmosphere

4.1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h

5.1: trifluoroacetic acid / dichloromethane / 1 h

6.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; 3.1: |Sonogashira Cross-Coupling;
DOI:10.1039/c3cc40628h