NH₂CH₂C₂HN₃CH₂C₆H₅PdCl₂

Base Information

• Chemical Name: NH₂CH₂C₂HN₃CH₂C₆H₅PdCl₂
• CAS No.: 1239917-90-8
• Molecular Formula: C₁₀H₁₂Cl₂N₄Pd
• Molecular Weight: 365.558
• Mol file: 1239917-90-8.mol

Synonyms:

Chemical Property of NH₂CH₂C₂HN₃CH₂C₆H₅PdCl₂

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of NH₂CH₂C₂HN₃CH₂C₆H₅PdCl₂

There total 1 articles about NH₂CH₂C₂HN₃CH₂C₆H₅PdCl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

potassium tetrachloropalladate(II) (10025-98-6) + 1-(1-benzyl-1H-[1,2,3]-triazol-4-yl)methylamine hydrochloride (852030-90-1) → NH2CH2C2HN3CH2C6H5PdCl2 (1239917-90-8)

Guidance literature:

In water; 1 equiv.of ligand in H2O added to soln. of K2PdCl4 in H2O, stirred for 24 h; filtered, washed (H2O, CH3OH, ether), dried (air);

DOI:10.1002/ejic.201000183

Reference yield:

NH2CH2C2HN3CH2C6H5PdCl2 (1239917-90-8) + silver nitrate + G (118-00-3) → (NH2C5H2N4OC4H4O(OH)2CH2OH)2Pd(NH2CH2C2HN3CH2C6H5)(2+)*2NO3(1-)=(NH2C5H2N4OC4H4O(OH)2CH2OH)2Pd(NH2CH2C2HN3CH2C6H5)(NO3)2

Guidance literature:

In water-d2; 1 equiv. of Pd complex stirred in D2O in the presence of 2.4 equiv. of AgNO3 in the dark for 2 d, filtered, treated with 2.5 equiv. of guanosine, stirred for 24 h; filtered, not isolated, detcd. by NMR;

DOI:10.1002/ejic.201000183

upstream raw materials:

potassium tetrachloropalladate(II)

1-(1-benzyl-1H-[1,2,3]-triazol-4-yl)methylamine hydrochloride