C₃₇H₄₅FN₆O₇

Base Information

Chemical Name:C₃₇H₄₅FN₆O₇
CAS No.:1338076-33-7
Molecular Formula:C₃₇H₄₅FN₆O₇
Molecular Weight:704.799
Hs Code.:

C<sub>37</sub>H<sub>45</sub>FN<sub>6</sub>O<sub>7</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₇H₄₅FN₆O₇

Chemical Property:

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Technology Process of C₃₇H₄₅FN₆O₇

There total 8 articles about C₃₇H₄₅FN₆O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1338075-08-3
C₁₃H₁₅FN₄O₃

: 1338076-33-7
C₃₇H₄₅FN₆O₇

Guidance literature:: Multi-step reaction with 4 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 5 h / 0 - 10 °C

2: 1-methyl-pyrrolidin-2-one / 120 °C / Molecular sieve

3: methanol / 0 - 15 °C

4: potassium carbonate / N,N-dimethyl-formamide / 10 °C

With di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; methanol; N,N-dimethyl-formamide; 1: Mitsunobu reaction;

Reference yield:

: 1338075-41-4
(4-fluoro-2-(4-methoxybenzyloxy)phenyl)methanol

: 1338076-33-7
C₃₇H₄₅FN₆O₇

Guidance literature:: Multi-step reaction with 5 steps

1.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 2 h / 0 - 20 °C

2.1: lithium hexamethyldisilazane / N,N-dimethyl-formamide; tetrahydrofuran / 0.5 h / 0 °C

2.2: 0 - 20 °C

3.1: 1-methyl-pyrrolidin-2-one / 120 °C / Molecular sieve

4.1: methanol / 0 - 15 °C

5.1: potassium carbonate / N,N-dimethyl-formamide / 10 °C

With carbon tetrabromide; potassium carbonate; triphenylphosphine; lithium hexamethyldisilazane; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 824-94-2
p-methoxybenzyl chloride

: 1338076-33-7
C₃₇H₄₅FN₆O₇

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium carbonate / acetonitrile / 12 h / Reflux

2.1: sodium tetrahydroborate / tetrahydrofuran / 0.25 h / 65 °C

2.2: 4.5 h / 65 °C

3.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 2 h / 0 - 20 °C

4.1: lithium hexamethyldisilazane / N,N-dimethyl-formamide; tetrahydrofuran / 0.5 h / 0 °C

4.2: 0 - 20 °C

5.1: 1-methyl-pyrrolidin-2-one / 120 °C / Molecular sieve

6.1: methanol / 0 - 15 °C

7.1: potassium carbonate / N,N-dimethyl-formamide / 10 °C

With sodium tetrahydroborate; carbon tetrabromide; potassium carbonate; triphenylphosphine; lithium hexamethyldisilazane; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;