potassium [N,N'-bis(2,6-diisopropylphenyl)-2,6-pyridinedicarboxamido-κ3N,N,N]nickel(II) chloride

Base Information

Chemical Name:potassium [N,N'-bis(2,6-diisopropylphenyl)-2,6-pyridinedicarboxamido-κ3N,N,N]nickel(II) chloride
CAS No.:864058-07-1
Molecular Formula:C₃₁H₃₇N₃O₂*Cl*K*Ni
Molecular Weight:616.895
Hs Code.:

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Chemical Property of potassium [N,N'-bis(2,6-diisopropylphenyl)-2,6-pyridinedicarboxamido-κ3N,N,N]nickel(II) chloride

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Technology Process of potassium [N,N'-bis(2,6-diisopropylphenyl)-2,6-pyridinedicarboxamido-κ3N,N,N]nickel(II) chloride

There total 1 articles about potassium [N,N'-bis(2,6-diisopropylphenyl)-2,6-pyridinedicarboxamido-κ3N,N,N]nickel(II) chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 29046-78-4
(1,2-dimethoxyethane)dichloronickel(II)

: dipotassium N,N'-bis(2,6-diisopropylphenyl)-2,6-pyridinedicarboxamidate

: 864058-07-1
potassium [N,N'-bis(2,6-diisopropylphenyl)-2,6-pyridinedicarboxamido-κ3N,N,N]nickel(II) chloride

Guidance literature:: In tetrahydrofuran; byproducts: KCl; (inert atm.); addn. of a slurry of nickel complex in THF to a soln. of potassium salt in THF, stirring for 3 h; filtration, drying in vac.; elem. anal.;
DOI:10.1021/om0501780

Reference yield:

: 864058-07-1
potassium [N,N'-bis(2,6-diisopropylphenyl)-2,6-pyridinedicarboxamido-κ3N,N,N]nickel(II) chloride

: 908094-04-2
phenyldiazomethane

: (benzylidene)(trimethylphosphine)[N,N'-bis(2,6-diisopropylphenyl)-2,6-pyridinedicarboxamido-κ3O,N,N]nickel(II)

: (benzylidene)(trimethylphosphine)[N,N'-bis(2,6-diisopropylphenyl)-2,6-pyridinedicarboxamido-κ3O,N,O]nickel(II)

Guidance literature:: In dichloromethane; (inert atm.); mixing diazo compd. with nickel complex in CH2Cl2 at -35°C, stirring for 5 min; evapn., trituration with pentane overnight, filtration, drying in vac.; obtained as a mixt. of isomers;
DOI:10.1021/om0501780