5α,10β,15α,20β-tetrakis(o-(R)-hydratropamidophenyl)porphyrin

Base Information

Chemical Name:5α,10β,15α,20β-tetrakis(o-(R)-hydratropamidophenyl)porphyrin
CAS No.:86457-67-2
Molecular Formula:C₈₀H₆₆N₈O₄
Molecular Weight:1203.46
Hs Code.:

Synonyms:

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Chemical Property of 5α,10β,15α,20β-tetrakis(o-(R)-hydratropamidophenyl)porphyrin

Chemical Property:

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Technology Process of 5α,10β,15α,20β-tetrakis(o-(R)-hydratropamidophenyl)porphyrin

There total 2 articles about 5α,10β,15α,20β-tetrakis(o-(R)-hydratropamidophenyl)porphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52199-35-6
tetrakis-5,10,15,20-(o-aminophenyl)porphyrin

: 25145-43-1,36240-11-6,59981-93-0,22414-26-2
2-phenylpropionyl chloride

: 86457-67-2,86495-89-8,86495-90-1
5α,10β,15α,20β-tetrakis(o-(R)-hydratropamidophenyl)porphyrin

: 86457-67-2,86495-89-8,86495-90-1
(S)-2-Phenyl-N-(2-{(1Z,4Z,9Z,15Z)-10,15,20-tris-[2-((S)-2-phenyl-propionylamino)-phenyl]-porphyrin-5-yl}-phenyl)-propionamide

Guidance literature:: In pyridine; dichloromethane; for 2h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/ja00356a016

Reference yield:

: 52199-35-6
tetrakis-5,10,15,20-(o-aminophenyl)porphyrin

: 25145-43-1,36240-11-6,59981-93-0,22414-26-2
2-phenylpropionyl chloride

: 86457-67-2,86495-89-8,86495-90-1
5α,10β,15α,20β-tetrakis(o-(R)-hydratropamidophenyl)porphyrin

: 86457-67-2,86495-89-8,86495-90-1
(S)-2-Phenyl-N-(2-{(1Z,4Z,9Z,15Z)-10,15,20-tris-[2-((S)-2-phenyl-propionylamino)-phenyl]-porphyrin-5-yl}-phenyl)-propionamide

Guidance literature:: In pyridine; dichloromethane; for 2h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/ja00356a016

Reference yield:

: 7647-01-0,15364-23-5
hydrogenchloride

: 86457-67-2
5α,10β,15α,20β-tetrakis(o-(R)-hydratropamidophenyl)porphyrin

: 7789-46-0
iron(II) bromide

: 86457-73-0
chloro[5α,10β,15α,20β-tetrakis(o-(R)-hydratropamidophenyl)porphyrinato]iron(III)

Guidance literature:: With 2,6-dimethylpyridine; In tetrahydrofuran; a soln. of FeBr2 and porphyrin was stirred at room temperature for 4 h under N2, exposed to air and stirred for further several hours; evapn., chromy. (basic alumina, chloroform), washing twice with 10% HCl, filtration through sodium chloride, evapn.; elem. anal.;
DOI:10.1021/ja00356a016