C₂₃H₃₃NOSi

Base Information

Chemical Name:C₂₃H₃₃NOSi
CAS No.:1393834-89-3
Molecular Formula:C₂₃H₃₃NOSi
Molecular Weight:367.607
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₃H₃₃NOSi

Chemical Property:

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Technology Process of C₂₃H₃₃NOSi

There total 4 articles about C₂₃H₃₃NOSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3376-24-7,68315-30-0
N-tert-butyl-α-phenylnitrone

: 1393834-75-7
2-(triethylsilyl)-6-(trimethylsilyl)phenyl triflate

: 1393834-89-3
C₂₃H₃₃NOSi

Guidance literature:: With cesium fluoride; In acetonitrile; at 23 ℃; for 22.5h; regioselective reaction; Inert atmosphere;
DOI:10.1021/ja306723r

Reference yield:

: 58144-49-3
2-bromo-6-(trimethylsilyl)phenol

: 1393834-89-3
C₂₃H₃₃NOSi

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1H-imidazole; dmap / neat (no solvent) / 4 h / 23 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 5.5 h / -78 °C / Inert atmosphere

3.1: n-butyllithium / hexane; diethyl ether / 1.67 h / 0 °C / Inert atmosphere

3.2: 0 - 23 °C / Inert atmosphere

4.1: cesium fluoride / acetonitrile / 22.5 h / 23 °C / Inert atmosphere

With 1H-imidazole; dmap; n-butyllithium; cesium fluoride; In tetrahydrofuran; diethyl ether; hexane; acetonitrile;
DOI:10.1021/ja306723r

Reference yield:

: 1393834-76-8
C₁₅H₂₇BrOSi₂

: 1393834-89-3
C₂₃H₃₃NOSi

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 5.5 h / -78 °C / Inert atmosphere

2.1: n-butyllithium / hexane; diethyl ether / 1.67 h / 0 °C / Inert atmosphere

2.2: 0 - 23 °C / Inert atmosphere

3.1: cesium fluoride / acetonitrile / 22.5 h / 23 °C / Inert atmosphere

With n-butyllithium; cesium fluoride; In tetrahydrofuran; diethyl ether; hexane; acetonitrile;
DOI:10.1021/ja306723r