2-[(η5-cyclopentadienyl)dicarbonyliron]-5-tert-butyl-1-[(phenylsulfonyl)iminomethyl]-1-cyclohexene

Base Information

Chemical Name:2-[(η5-cyclopentadienyl)dicarbonyliron]-5-tert-butyl-1-[(phenylsulfonyl)iminomethyl]-1-cyclohexene
CAS No.:299915-35-8
Molecular Formula:C₂₄H₂₇FeNO₄S
Molecular Weight:481.396
Hs Code.:

Synonyms:

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Chemical Property of 2-[(η5-cyclopentadienyl)dicarbonyliron]-5-tert-butyl-1-[(phenylsulfonyl)iminomethyl]-1-cyclohexene

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Technology Process of 2-[(η5-cyclopentadienyl)dicarbonyliron]-5-tert-butyl-1-[(phenylsulfonyl)iminomethyl]-1-cyclohexene

There total 1 articles about 2-[(η5-cyclopentadienyl)dicarbonyliron]-5-tert-butyl-1-[(phenylsulfonyl)iminomethyl]-1-cyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-10-2
benzenesulfonamide

: 224454-49-3
C₆H₇(C(CH₃)3)(Fe(CO)2(C₅H₅))(CHO)

: 299915-35-8
2-[(η5-cyclopentadienyl)dicarbonyliron]-5-tert-butyl-1-[(phenylsulfonyl)iminomethyl]-1-cyclohexene

Guidance literature:: With (C₂H₅)3N; TiCl₄; In dichloromethane; under Ar; to a soln. of Fe complex and C6H5SO2NH2 in CH2Cl2 was added (C2H5)3N and TiCl4 at 0°C, the light-protected mixt. was stirred for 5 min, then the mixt. was stirred at 25°C for 5 h; the mixt. was added to a NH4Cl aq. soln., the org. phase was washed with HCl, the aq. layer was extd. with CH2Cl2, washed with brine, dried with MgSO4, the solvent was removed in vac.; elem. anal.;
DOI:10.1021/om000235j

Reference yield:

: 109-72-8
n-butyllithium

: 299915-35-8
2-[(η5-cyclopentadienyl)dicarbonyliron]-5-tert-butyl-1-[(phenylsulfonyl)iminomethyl]-1-cyclohexene

: [(η5-cyclopentadienyl)(carbonyl)Fe(CON(SO2C6H5)CH(C4H9)(C6H7C(CH3)3))](1-)

Guidance literature:: under Ar; to a light-protected soln. of the N-sulfonyl imine in THF wasadded C4H9Li; not isolated, detected by IR;
DOI:10.1021/om000235j