C₂₅H₂₂FN₃O₂S

Base Information

Chemical Name:C₂₅H₂₂FN₃O₂S
CAS No.:1356679-28-1
Molecular Formula:C₂₅H₂₂FN₃O₂S
Molecular Weight:447.533
Hs Code.:

C<sub>25</sub>H<sub>22</sub>FN<sub>3</sub>O<sub>2</sub>S

Synonyms:

Suppliers and Price of C₂₅H₂₂FN₃O₂S

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₅H₂₂FN₃O₂S

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₅H₂₂FN₃O₂S

There total 8 articles about C₂₅H₂₂FN₃O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1356679-50-9
N-(4-bromo-2-fluorophenyl)-4-(1,3-dioxan-2-yl)-2-fluorobenzothioamide

: 1356679-28-1
C₂₅H₂₂FN₃O₂S

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium carbonate / N,N-dimethyl-formamide / 110 °C / Inert atmosphere

2.1: palladium diacetate; caesium carbonate; triphenylphosphine / toluene / 120 °C

3.1: lithium hexamethyldisilazane / tetrahydrofuran

4.1: hydrogenchloride; water / tetrahydrofuran / 65 °C

5.1: sodium cyanoborohydride; acetic acid; N-ethyl-N,N-diisopropylamine / methanol; dichloromethane

6.1: water; sodium hydroxide / tetrahydrofuran

6.2: pH 6 / aq. phosphate buffer

With hydrogenchloride; water; palladium diacetate; sodium cyanoborohydride; sodium carbonate; caesium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; triphenylphosphine; sodium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmcl.2011.10.069

Reference yield:

: 1202076-30-9
2-(4-(1,3-dioxan-2-yl)-2-fluorophenyl)-6-bromobenzo[d]thiazole

: 1356679-28-1
C₂₅H₂₂FN₃O₂S

Guidance literature:: Multi-step reaction with 5 steps

1.1: palladium diacetate; caesium carbonate; triphenylphosphine / toluene / 120 °C

2.1: lithium hexamethyldisilazane / tetrahydrofuran

3.1: hydrogenchloride; water / tetrahydrofuran / 65 °C

4.1: sodium cyanoborohydride; acetic acid; N-ethyl-N,N-diisopropylamine / methanol; dichloromethane

5.1: water; sodium hydroxide / tetrahydrofuran

5.2: pH 6 / aq. phosphate buffer

With hydrogenchloride; water; palladium diacetate; sodium cyanoborohydride; caesium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; triphenylphosphine; sodium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1016/j.bmcl.2011.10.069

Reference yield:

: 1356679-18-9
C₂₃H₁₉FN₂O₂S

: 1356679-28-1
C₂₅H₂₂FN₃O₂S

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran

2.1: hydrogenchloride; water / tetrahydrofuran / 65 °C

3.1: sodium cyanoborohydride; acetic acid; N-ethyl-N,N-diisopropylamine / methanol; dichloromethane

4.1: water; sodium hydroxide / tetrahydrofuran

4.2: pH 6 / aq. phosphate buffer

With hydrogenchloride; water; sodium cyanoborohydride; acetic acid; N-ethyl-N,N-diisopropylamine; sodium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.bmcl.2011.10.069