[Ru(η5-C5H5)(triphenylstibine)(κ2-pyridine-2-carbaldehyde azine)]BF4

Base Information

• Chemical Name: [Ru(η5-C5H5)(triphenylstibine)(κ2-pyridine-2-carbaldehyde azine)]BF4
• CAS No.: 799293-38-2
• Molecular Formula: BF₄*C₃₅H₃₀N₄RuSb
• Molecular Weight: 816.275
• Mol file: 799293-38-2.mol

Synonyms:

Chemical Property of [Ru(η5-C5H5)(triphenylstibine)(κ2-pyridine-2-carbaldehyde azine)]BF4

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of [Ru(η5-C5H5)(triphenylstibine)(κ2-pyridine-2-carbaldehyde azine)]BF4

There total 1 articles about [Ru(η5-C5H5)(triphenylstibine)(κ2-pyridine-2-carbaldehyde azine)]BF4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

ammonium tetrafluroborate (13826-83-0) + (η5-C5H5)RuCl(SbPh3)2 + 2-pyridinecarbaldehyde azine (6957-24-0) → [Ru(η5-C5H5)(triphenylstibine)(κ2-pyridine-2-carbaldehyde azine)]BF4 (799293-38-2)

Guidance literature:

In methanol; under N2; suspn. of Ru complex in MeOH treated with ligand (2 equiv.); heated under reflux for ca. 10 h; cooled to room temp.; filtered through Celite; satd. soln. of NH4BF4 in MeOH added to filtrate; elem. anal.;

DOI:10.1016/j.jorganchem.2004.08.026

upstream raw materials:

ammonium tetrafluroborate

2-pyridinecarbaldehyde azine