Cu(II)-5-(1,5-dihydroxypent-3-yl)-15-phenylporphyrin

Base Information

Chemical Name:Cu(II)-5-(1,5-dihydroxypent-3-yl)-15-phenylporphyrin
CAS No.:1021946-43-9
Molecular Formula:C₃₁H₂₆CuN₄O₂
Molecular Weight:550.119
Hs Code.:

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Chemical Property of Cu(II)-5-(1,5-dihydroxypent-3-yl)-15-phenylporphyrin

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Technology Process of Cu(II)-5-(1,5-dihydroxypent-3-yl)-15-phenylporphyrin

There total 1 articles about Cu(II)-5-(1,5-dihydroxypent-3-yl)-15-phenylporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 5-(1,5-dihydroxypent-3-yl)-15-phenylprophyrin

: 142-71-2
copper diacetate

: 1021946-43-9
Cu(II)-5-(1,5-dihydroxypent-3-yl)-15-phenylporphyrin

Guidance literature:: In methanol; chloroform; porphyrin in CHCl3-MeOH treated with Cu acetate (10 equiv.); stirred at room temp. for 12 h; diluted with ethyl acetate and H2O; aq. layer extd. with ethyl acetate; org. layer dried (Na2SO4); chromd. (neutral alumina, CH2Cl2 to CH2Cl2-MeOH-THF 5:1:1);
DOI:10.1039/b714127k

Reference yield: 35.0%

: 1021946-43-9
Cu(II)-5-(1,5-dihydroxypent-3-yl)-15-phenylporphyrin

: 813-77-4
Dimethyl chlorophosphate

: 1021946-44-0
Cu(II)-5-[1,5-bis(dimethoxyphosphoryloxy)pent-3-yl]-15-phenylporphyrin

Guidance literature:: With dmap; In dichloromethane; under Ar; soln. of Cu porphyrin in dry CH2Cl2 treated with DMAP (10 equiv.); stirred at room temp. for 10 min; ClP(O)(OMe)2 added dropwise; stirred at room temp. for 12 h; column chromd. (silica, CH2Cl2 to CH2Cl2-MeOH 97:3);
DOI:10.1039/b714127k