(η(6)-azoxybenzene)(η(5)-2,4-cyclopentadien-1-yl)ruthenium hexafluorophosphate

Base Information

• Chemical Name: (η(6)-azoxybenzene)(η(5)-2,4-cyclopentadien-1-yl)ruthenium hexafluorophosphate
• CAS No.: 174499-37-7
• Molecular Formula: C₁₇H₁₅N₂ORu*F₆P
• Molecular Weight: 509.353
• Mol file: 174499-37-7.mol

Synonyms:

Chemical Property of (η(6)-azoxybenzene)(η(5)-2,4-cyclopentadien-1-yl)ruthenium hexafluorophosphate

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of (η(6)-azoxybenzene)(η(5)-2,4-cyclopentadien-1-yl)ruthenium hexafluorophosphate

There total 1 articles about (η(6)-azoxybenzene)(η(5)-2,4-cyclopentadien-1-yl)ruthenium hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

cyclopentadienylruthenium(II) trisacetonitrile hexafluorophosphate + azoxybenzene (495-48-7,55599-32-1) → (η(6)-azoxybenzene)(η(5)-2,4-cyclopentadien-1-yl)ruthenium hexafluorophosphate (174499-37-7)

Guidance literature:

In dichloromethane; N2-atmosphere; refluxing Ru-complex with excess of azoxybenzene for 15 h; chromy., crystn. (Me2CO/Et2O); elem. anal.;

DOI:10.1016/0022-328X(95)05717-4

upstream raw materials:

azoxybenzene

Refernces