C₅₉H₈₀N₆O₁₆S₂

Base Information

Chemical Name:C₅₉H₈₀N₆O₁₆S₂
CAS No.:1356846-31-5
Molecular Formula:C₅₉H₈₀N₆O₁₆S₂
Molecular Weight:1193.45
Hs Code.:

C<sub>59</sub>H<sub>80</sub>N<sub>6</sub>O<sub>16</sub>S<sub>2</sub>

Synonyms:

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Chemical Property of C₅₉H₈₀N₆O₁₆S₂

Chemical Property:

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Technology Process of C₅₉H₈₀N₆O₁₆S₂

There total 7 articles about C₅₉H₈₀N₆O₁₆S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₉H₆₆N₄O₁₄S

: 58-85-5,22879-79-4
biotin

: 1356846-31-5
C₅₉H₈₀N₆O₁₆S₂

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1021/ja209641t

Reference yield:

: 1356846-55-3
C₁₉H₁₉ClN₂O₅S

: 1356846-31-5
C₅₉H₈₀N₆O₁₆S₂

Guidance literature:: Multi-step reaction with 5 steps

1: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Inert atmosphere

2: palladium on activated charcoal; hydrogen / methanol / 5 h / 20 °C

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere

4: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

5: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere

With dmap; palladium on activated charcoal; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja209641t

Reference yield:

: 1356846-56-4
C₃₀H₄₁N₃O₁₀S

: 1356846-31-5
C₅₉H₈₀N₆O₁₆S₂

Guidance literature:: Multi-step reaction with 4 steps

1: palladium on activated charcoal; hydrogen / methanol / 5 h / 20 °C

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere

3: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere

With palladium on activated charcoal; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja209641t