C₂₄H₂₈N₂O₃S₂

Base Information

Chemical Name:C₂₄H₂₈N₂O₃S₂
CAS No.:1374354-89-8
Molecular Formula:C₂₄H₂₈N₂O₃S₂
Molecular Weight:456.63
Hs Code.:

C<sub>24</sub>H<sub>28</sub>N<sub>2</sub>O<sub>3</sub>S<sub>2</sub>

Synonyms:

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Chemical Property of C₂₄H₂₈N₂O₃S₂

Chemical Property:

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Technology Process of C₂₄H₂₈N₂O₃S₂

There total 17 articles about C₂₄H₂₈N₂O₃S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1374354-76-3
C₁₆H₂₉NO₃SSi

: 1374354-89-8
C₂₄H₂₈N₂O₃S₂

Guidance literature:: Multi-step reaction with 11 steps

1: diethyl ether

2: sodium hexamethyldisilazane; triethylamine / tetrahydrofuran

3: N-Bromosuccinimide / tetrahydrofuran

4: sodium diformamide / acetonitrile

5: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane

6: 1H-imidazole / N,N-dimethyl-formamide

7: Lawessons reagent; pyridine / toluene / 100 °C

8: tetrabutyl ammonium fluoride / tetrahydrofuran

9: thionyl chloride / toluene

10: N-ethyl-N,N-diisopropylamine / acetonitrile

11: water; sodium hydroxide / ethanol

With Lawessons reagent; pyridine; 1H-imidazole; N-Bromosuccinimide; thionyl chloride; sodium diformamide; tetrabutyl ammonium fluoride; water; sodium hexamethyldisilazane; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067

Reference yield:

: 185147-08-4
4-fluoro-3-methylbenzonitrile

: 1374354-89-8
C₂₄H₂₈N₂O₃S₂

Guidance literature:: Multi-step reaction with 9 steps

1: sodium hydride

2: sodium hydroxide

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane

4: 1H-imidazole / N,N-dimethyl-formamide

5: Lawessons reagent; pyridine / toluene / 100 °C

6: tetrabutyl ammonium fluoride / tetrahydrofuran

7: thionyl chloride / toluene

8: N-ethyl-N,N-diisopropylamine / acetonitrile

9: water; sodium hydroxide / ethanol

With Lawessons reagent; pyridine; 1H-imidazole; thionyl chloride; tetrabutyl ammonium fluoride; water; sodium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067

Reference yield:

: 230623-72-0
(4-bromo-thiophene-2-ylmethoxy)-tert-butyl-dimethylsilane

: 1374354-89-8
C₂₄H₂₈N₂O₃S₂

Guidance literature:: Multi-step reaction with 14 steps

1: 1,3-bis[(diphenylphosphino)propane]dichloronickel(II)

2: n-butyllithium / tetrahydrofuran

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane

4: diethyl ether

5: sodium hexamethyldisilazane; triethylamine / tetrahydrofuran

6: N-Bromosuccinimide / tetrahydrofuran

7: sodium diformamide / acetonitrile

8: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane

9: 1H-imidazole / N,N-dimethyl-formamide

10: Lawessons reagent; pyridine / toluene / 100 °C

11: tetrabutyl ammonium fluoride / tetrahydrofuran

12: thionyl chloride / toluene

13: N-ethyl-N,N-diisopropylamine / acetonitrile

14: water; sodium hydroxide / ethanol

With Lawessons reagent; pyridine; 1H-imidazole; N-Bromosuccinimide; n-butyllithium; thionyl chloride; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); sodium diformamide; tetrabutyl ammonium fluoride; water; sodium hexamethyldisilazane; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067