(3R,5R)-3-tert-Butoxycarbonylamino-5-(tert-butyl-dimethyl-silanyloxy)-6-((2E,4Z)-hexa-2,4-dienoylamino)-hexanoic acid pentafluorophenyl ester

Base Information

Chemical Name:(3R,5R)-3-tert-Butoxycarbonylamino-5-(tert-butyl-dimethyl-silanyloxy)-6-((2E,4Z)-hexa-2,4-dienoylamino)-hexanoic acid pentafluorophenyl ester
CAS No.:871506-36-4
Molecular Formula:C₂₉H₄₁F₅N₂O₆Si
Molecular Weight:636.732
Hs Code.:

(3R,5R)-3-tert-Butoxycarbonylamino-5-(tert-butyl-dimethyl-silanyloxy)-6-((2E,4Z)-hexa-2,4-dienoylamino)-hexanoic acid pentafluorophenyl ester

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Chemical Property of (3R,5R)-3-tert-Butoxycarbonylamino-5-(tert-butyl-dimethyl-silanyloxy)-6-((2E,4Z)-hexa-2,4-dienoylamino)-hexanoic acid pentafluorophenyl ester

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Technology Process of (3R,5R)-3-tert-Butoxycarbonylamino-5-(tert-butyl-dimethyl-silanyloxy)-6-((2E,4Z)-hexa-2,4-dienoylamino)-hexanoic acid pentafluorophenyl ester

There total 8 articles about (3R,5R)-3-tert-Butoxycarbonylamino-5-(tert-butyl-dimethyl-silanyloxy)-6-((2E,4Z)-hexa-2,4-dienoylamino)-hexanoic acid pentafluorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 871506-31-9
3-tert-butoxycarbonylamino-5-(tert-butyl-dimethyl-silanyloxy)-6-nitro-hexanoic acid

: 871506-36-4
(3R,5R)-3-tert-Butoxycarbonylamino-5-(tert-butyl-dimethyl-silanyloxy)-6-((2E,4Z)-hexa-2,4-dienoylamino)-hexanoic acid pentafluorophenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / HCO₂NH₄ / Pd/C / methanol / 20 °C

2: 71 percent / Et₃N / dimethylformamide / 20 °C

3: EDC / CH₂Cl₂ / 20 °C

With ammonium formate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-2005-917106

Reference yield:

: 871506-35-3
(3R,5R)-3-tert-Butoxycarbonylamino-5-(tert-butyl-dimethyl-silanyloxy)-6-((2E,4Z)-hexa-2,4-dienoylamino)-hexanoic acid

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 871506-36-4
(3R,5R)-3-tert-Butoxycarbonylamino-5-(tert-butyl-dimethyl-silanyloxy)-6-((2E,4Z)-hexa-2,4-dienoylamino)-hexanoic acid pentafluorophenyl ester

Guidance literature:: With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; at 20 ℃;
DOI:10.1055/s-2005-917106

Reference yield:

: 871506-32-0
(2E,4Z)-2,4-hexadienoic acid pentafluorophenyl ester

: 871506-36-4
(3R,5R)-3-tert-Butoxycarbonylamino-5-(tert-butyl-dimethyl-silanyloxy)-6-((2E,4Z)-hexa-2,4-dienoylamino)-hexanoic acid pentafluorophenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / Et₃N / dimethylformamide / 20 °C

2: EDC / CH₂Cl₂ / 20 °C

With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-2005-917106