C₃₂H₃₂ClFN₄O₉S

Base Information

Chemical Name:C₃₂H₃₂ClFN₄O₉S
CAS No.:1417792-25-6
Molecular Formula:C₃₂H₃₂ClFN₄O₉S
Molecular Weight:703.145
Hs Code.:

C<sub>32</sub>H<sub>32</sub>ClFN<sub>4</sub>O<sub>9</sub>S

Synonyms:

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Chemical Property of C₃₂H₃₂ClFN₄O₉S

Chemical Property:

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Technology Process of C₃₂H₃₂ClFN₄O₉S

There total 11 articles about C₃₂H₃₂ClFN₄O₉S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₃H₃₃ClFN₃O₁₀S

: 1417792-25-6
C₃₂H₃₂ClFN₄O₉S

Guidance literature:: With water; potassium carbonate; In methanol; at 80 ℃; for 0.0833333h;
DOI:10.1021/jm3014844

Reference yield:

: C₂₈H₃₁ClFN₃O₉S

: 1417792-25-6
C₃₂H₃₂ClFN₄O₉S

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 0.08 h / 100 °C

2: potassium carbonate; water / methanol / 0.08 h / 80 °C

With water; potassium carbonate; triethylamine; In tetrahydrofuran; methanol;
DOI:10.1021/jm3014844

Reference yield:

: 2,3:4,5-bis-O-(1-methylethylidene)-D-mannitol

: 1417792-25-6
C₃₂H₃₂ClFN₄O₉S

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 20 °C

1.2: 0.25 h / 60 °C

2.1: dipyridinium dichromate / dichloromethane / 2 h / 20 °C / Molecular sieve

3.1: dichloromethane

4.1: dichloromethane / 0.08 h / Molecular sieve

5.1: sodium tris(acetoxy)borohydride / dichloromethane / 2 h / 20 °C

6.1: zinc; ammonium chloride / water; acetone / 0.17 h / 20 °C

7.1: hydrogenchloride / methanol / 0.17 h / 60 °C

8.1: triethylamine / tetrahydrofuran / 0 °C

9.1: triethylamine / tetrahydrofuran / 0.08 h / 100 °C

10.1: potassium carbonate; water / methanol / 0.08 h / 80 °C

With hydrogenchloride; dipyridinium dichromate; water; sodium tris(acetoxy)borohydride; sodium hydride; potassium carbonate; ammonium chloride; triethylamine; zinc; In tetrahydrofuran; methanol; dichloromethane; water; acetone; mineral oil;
DOI:10.1021/jm3014844