(R)-2-(1-(4-methoxyphenyl)-1,2,3,4-tetrahydronaphthalen-1-yl)ethanol

Base Information

Chemical Name:(R)-2-(1-(4-methoxyphenyl)-1,2,3,4-tetrahydronaphthalen-1-yl)ethanol
CAS No.:1579249-96-9
Molecular Formula:C₁₉H₂₂O₂
Molecular Weight:282.382
Hs Code.:

Synonyms:

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Chemical Property of (R)-2-(1-(4-methoxyphenyl)-1,2,3,4-tetrahydronaphthalen-1-yl)ethanol

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Technology Process of (R)-2-(1-(4-methoxyphenyl)-1,2,3,4-tetrahydronaphthalen-1-yl)ethanol

There total 5 articles about (R)-2-(1-(4-methoxyphenyl)-1,2,3,4-tetrahydronaphthalen-1-yl)ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 1579249-94-7
(R)-1-ethenyl-1-(4-methoxyphenyl)-1,2,3,4-tetrahydronaphthalene

: 1579249-96-9
(R)-2-(1-(4-methoxyphenyl)-1,2,3,4-tetrahydronaphthalen-1-yl)ethanol

Guidance literature:: (R)-1-ethenyl-1-(4-methoxyphenyl)-1,2,3,4-tetrahydronaphthalene; With dimethylsulfide borane complex; In tetrahydrofuran; at 0 - 20 ℃; for 1h;

With dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; water; at 0 - 20 ℃; for 1h;
DOI:10.1021/jo500068p

Reference yield:

: 529-34-0
3,4-dihydronaphthalene-1(2H)-one

: 1579249-96-9
(R)-2-(1-(4-methoxyphenyl)-1,2,3,4-tetrahydronaphthalen-1-yl)ethanol

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / mineral oil; tetrahydrofuran / 1 h / 0 °C

1.2: 24 h / 20 °C

2.1: diisobutylaluminium hydride / hexane; toluene / 12 h / -78 - 20 °C

3.1: dmap; triethylamine / dichloromethane / 20 h / 0 - 20 °C

4.1: 1-((1S,2S)-2-hydroxyindan-1-yl)-3-pentamethylphenylimidazolinium hexafluorophosphate; copper(l) chloride; sodium methylate / tetrahydrofuran / 0.08 h / 20 °C

4.2: 60 h / 20 °C

5.1: dimethylsulfide borane complex / tetrahydrofuran / 1 h / 0 - 20 °C

5.2: 1 h / 0 - 20 °C

With dmap; dimethylsulfide borane complex; 1-((1S,2S)-2-hydroxyindan-1-yl)-3-pentamethylphenylimidazolinium hexafluorophosphate; sodium methylate; sodium hydride; diisobutylaluminium hydride; triethylamine; copper(l) chloride; In tetrahydrofuran; hexane; dichloromethane; toluene; mineral oil;
DOI:10.1021/jo500068p

Reference yield:

: 1579250-10-4
diethyl (E)-2-(3,4-dihydronaphthalen-1(2H)-ylidene)ethyl phosphate

: 1579249-96-9
(R)-2-(1-(4-methoxyphenyl)-1,2,3,4-tetrahydronaphthalen-1-yl)ethanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1-((1S,2S)-2-hydroxyindan-1-yl)-3-pentamethylphenylimidazolinium hexafluorophosphate; copper(l) chloride; sodium methylate / tetrahydrofuran / 0.08 h / 20 °C

1.2: 60 h / 20 °C

2.1: dimethylsulfide borane complex / tetrahydrofuran / 1 h / 0 - 20 °C

2.2: 1 h / 0 - 20 °C

With dimethylsulfide borane complex; 1-((1S,2S)-2-hydroxyindan-1-yl)-3-pentamethylphenylimidazolinium hexafluorophosphate; sodium methylate; copper(l) chloride; In tetrahydrofuran;
DOI:10.1021/jo500068p