C₉H₁₈O₅

Base Information

• Chemical Name: C₉H₁₈O₅
• CAS No.: 1286272-49-8
• Molecular Formula: C₉H₁₈O₅
• Molecular Weight: 206.239
• Mol file: 1286272-49-8.mol

Synonyms:

Chemical Property of C₉H₁₈O₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₉H₁₈O₅

There total 6 articles about C₉H₁₈O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.5%

1,1,1-tri(hydroxymethyl)propane (77-99-6) + Diethyl carbonate (105-58-8,76619-83-5) → trimethylolpropane cyclic monocarbonate (38802-97-0) + C9H18O5 (1286272-49-8) + C12H22O7 (1286272-50-1)

Guidance literature:

With Novozym₄₃₅; at 60 ℃; for 48h; Molecular sieve; Enzymatic reaction; neat (no solvent);

DOI:10.1039/c0gc00783h

Reference yield: 71.5%

1,1,1-tri(hydroxymethyl)propane (77-99-6) + Diethyl carbonate (105-58-8,76619-83-5) → trimethylolpropane cyclic monocarbonate (38802-97-0) + C9H18O5 (1286272-49-8) + C10H16O6 (282098-17-3) + C12H22O7 (1286272-50-1)

Guidance literature:

With Novozym₄₃₅; at 60 ℃; for 120h; Molecular sieve; Enzymatic reaction; neat (no solvent);

DOI:10.1039/c0gc00783h

Reference yield: 71.5%

→ trimethylolpropane cyclic monocarbonate (38802-97-0) + C9H18O5 (1286272-49-8)

Guidance literature:

Product distribution / selectivity;

upstream raw materials:

1,1,1-tri(hydroxymethyl)propane

Diethyl carbonate

Refernces

• 1、 -. "SOLVENT-FREE SYNTHESIS OF CYCLIC CARBONATES". Page/Page column 6. . Retrieved 2012/01/06.