fac-{W(CO)3(NCEt)(N,N'-dicyclohexylethylenediimine)}

Base Information

Chemical Name:fac-{W(CO)3(NCEt)(N,N'-dicyclohexylethylenediimine)}
CAS No.:103947-73-5
Molecular Formula:C₂₀H₂₉N₃O₃W
Molecular Weight:543.319
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of fac-{W(CO)3(NCEt)(N,N'-dicyclohexylethylenediimine)}

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Technology Process of fac-{W(CO)3(NCEt)(N,N'-dicyclohexylethylenediimine)}

There total 1 articles about fac-{W(CO)3(NCEt)(N,N'-dicyclohexylethylenediimine)} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: N,N'-di-cyclohexyl-1,4-diazabuta-1,3-diene

: 83732-33-6,84580-21-2
fac-{W(CO)3(C₂H₅CN)3}

: 103947-73-5
fac-{W(CO)3(NCEt)(N,N'-dicyclohexylethylenediimine)}

Guidance literature:: In dichloromethane; charging three-necked flask with W(CO)3(NCC2H5)3 (4.62 mmol) and C6H11NCHCHNC6H11 (5.08 mmol); addn. of CH2Cl2 by syringe; stirring vigorously under N2 for 2 h at ambient temp.;; filtering, evapg filtrate to dryness under a stream of N2; recrystn. from propionitrile/petroleum ether; elem. anal.;;
DOI:10.1016/S0277-5387(00)84447-2

Reference yield: 94.0%

: 103947-73-5
fac-{W(CO)3(NCEt)(N,N'-dicyclohexylethylenediimine)}

: 119072-54-7,2769-71-3
2,6-dimethylphenyl isonitrile

: 103947-80-4
fac-{W(CO)3(2,6-dimethylphenyl isocyanide)(N,N'-dicyclohexylethylenediimine)}

Guidance literature:: In dichloromethane; stirring W(CO)3(NCC2H5)(C6H11NCHCHNC6H11) (1.08 mmol) in dry deoxygenated CH2Cl2 at room temp.; addn. of 2,6-dimethylphenyl isocyanide (1.08 mmol); stirring mixt. at room temp. for 6 h;; evapg. to dryness under reduced pressure; washing with copious amts. of petroleum ether; recrystn. from acetone/diethyl ether;;
DOI:10.1016/S0277-5387(00)84447-2

Reference yield: 91.0%

: 103947-73-5
fac-{W(CO)3(NCEt)(N,N'-dicyclohexylethylenediimine)}

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 103947-76-8
fac-{W(CO)3(tert-butyl isocyanide)(N,N'-dicyclohexylethylenediimine)}

Guidance literature:: In dichloromethane; stirring W(CO)3(NCC2H5)(C6H11NCHCHNC6H11) (1.08 mmol) in dry deoxygenated CH2Cl2 at room temp.; addn. of tert-butyl isocyanide (1.08 mmol); stirring mixt. at room temp. for 6 h;; evapg. to dryness under reduced pressure; washing with copious amts. of petroleum ether; recrystn. from acetone/diethyl ether;;
DOI:10.1016/S0277-5387(00)84447-2