[C₆H₄CH(CH₃)2N]2C₁₂H₆NiBr₂

Base Information

Chemical Name:[C₆H₄CH(CH₃)2N]2C₁₂H₆NiBr₂
CAS No.:439607-71-3
Molecular Formula:C₃₀H₂₈Br₂N₂Ni
Molecular Weight:635.064
Hs Code.:

[C<sub>6</sub>H<sub>4</sub>CH(CH<sub>3</sub>)2N]2C<sub>12</sub>H<sub>6</sub>NiBr<sub>2</sub>

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Chemical Property of [C₆H₄CH(CH₃)2N]2C₁₂H₆NiBr₂

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Technology Process of [C₆H₄CH(CH₃)2N]2C₁₂H₆NiBr₂

There total 2 articles about [C₆H₄CH(CH₃)2N]2C₁₂H₆NiBr₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 28923-39-9
nickel(II) bromide dimethoxyethane

: 439607-72-4
N,N'-bis(2-isopropylphenyl)acenaphthenequinonediimine

: 439607-71-3
[C₆H₄CH(CH₃)2N]2C₁₂H₆NiBr₂

Guidance literature:: In dichloromethane; (Ar); mixt. of Ni salt and the ligand stirred in CH2Cl2 at room temp. for 16 h; the suspn. filtered, the filtrate collected, the solvent removed, the residue washed with ether;
DOI:10.1016/S0022-328X(01)01340-7

Reference yield: 72.0%

: 643-28-7
2-isopropylaniline

: 13462-88-9
nickel dibromide

: 82-86-0
acenaphthene quinone

: 439607-71-3
[C₆H₄CH(CH₃)2N]2C₁₂H₆NiBr₂

Guidance literature:: In acetic acid; (Ar); to soln. of quinone in glacial acetic acid at 50°C aniline added; this mixt. warmed to 120°C, refluxed for 4 h; Ni salt added and the mixt refluxed for 16 h; the solvent removed in vac., the solid washed 3 times with ether, or alternatively by Soxhlet extn.; the residue extd. with CH2Cl2, filtered; this process repeated twice, solvent removed in vac.;
DOI:10.1016/S0022-328X(01)01340-7