(((C₅H₄CH₃)MoS₂)2CH₂CCC₆H₅)2

Base Information

• Chemical Name: (((C₅H₄CH₃)MoS₂)2CH₂CCC₆H₅)2
• CAS No.: 864448-63-5
• Molecular Formula: C₄₂H₄₂Mo₄S₈
• Molecular Weight: 1187.08

Synonyms:

Chemical Property of (((C₅H₄CH₃)MoS₂)2CH₂CCC₆H₅)2

Chemical Property:

Purity/Quality:

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Technology Process of (((C₅H₄CH₃)MoS₂)2CH₂CCC₆H₅)2

There total 1 articles about (((C₅H₄CH₃)MoS₂)2CH₂CCC₆H₅)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

{MeCpMo(μ-S)}2(.mu-S2CH2) + 1,4-diphenyl-1,3-butadiyne (886-66-8) → (((C5H4CH3)MoS2)2CH2CCC6H5)2 (864448-63-5)

Guidance literature:

In tetrahydrofuran; under N2 atm. (MeCpMoμ-S)2S2CH2 and 1,4-diphenylbutadiyne (2:1) in THF were stirred for 1 h; solvent was removed in vacuo, residue was recrystd. by layering Et2O into CH2Cl2 soln.; elem. anal.;

DOI:10.1021/om050317d

Reference yield: 33.0%

(((C5H4CH3)MoS2)2CH2CCC6H5)2 (864448-63-5) + trifluorormethanesulfonic acid (1493-13-6) → ((((C5H4CH3)MoS2)2CH2CCC6H5)2)(2+)*2CF3SO3(1-)=((((C5H4CH3)MoS2)2CH2CCC6H5)2)(CF3SO3)2

Guidance literature:

In dichloromethane; under N2 atm. soln. Mo complex and CF3SO3H in CH2Cl2 were stirred for 3 days; ppt. was filtered and recrystd. by dissolving in MeCN and letting ET2O slowly diffuse into the soln.;

DOI:10.1021/om050317d

upstream raw materials:

1,4-diphenyl-1,3-butadiyne

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