tert-butyl N-2-{2-[2-(3-{[2-(4-methoxyphenyl)-1-oxo-1H,2H-[1,2,4]triazolo[4,3-a]quinoxalin-4-yl]carbamoyl}propanamido)ethoxy]ethoxy}ethyl carbamate

Base Information

Chemical Name:tert-butyl N-2-{2-[2-(3-{[2-(4-methoxyphenyl)-1-oxo-1H,2H-[1,2,4]triazolo[4,3-a]quinoxalin-4-yl]carbamoyl}propanamido)ethoxy]ethoxy}ethyl carbamate
CAS No.:1359959-28-6
Molecular Formula:C₃₁H₃₉N₇O₈
Molecular Weight:637.693
Hs Code.:

tert-butyl N-2-{2-[2-(3-{[2-(4-methoxyphenyl)-1-oxo-1H,2H-[1,2,4]triazolo[4,3-a]quinoxalin-4-yl]carbamoyl}propanamido)ethoxy]ethoxy}ethyl carbamate

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Chemical Property of tert-butyl N-2-{2-[2-(3-{[2-(4-methoxyphenyl)-1-oxo-1H,2H-[1,2,4]triazolo[4,3-a]quinoxalin-4-yl]carbamoyl}propanamido)ethoxy]ethoxy}ethyl carbamate

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Technology Process of tert-butyl N-2-{2-[2-(3-{[2-(4-methoxyphenyl)-1-oxo-1H,2H-[1,2,4]triazolo[4,3-a]quinoxalin-4-yl]carbamoyl}propanamido)ethoxy]ethoxy}ethyl carbamate

There total 2 articles about tert-butyl N-2-{2-[2-(3-{[2-(4-methoxyphenyl)-1-oxo-1H,2H-[1,2,4]triazolo[4,3-a]quinoxalin-4-yl]carbamoyl}propanamido)ethoxy]ethoxy}ethyl carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 749248-72-4
3-({2-[2-(2-{[(tert-butoxy)carbonyl]amino}ethoxy)ethoxy]ethyl}carbamoyl)propanoic acid

: 269716-68-9
4-amino-2-(4-methoxyphenyl)-1,2,4-triazolo[4,3-a]quinoxalin-1-one

: 1359959-28-6
tert-butyl N-2-{2-[2-(3-{[2-(4-methoxyphenyl)-1-oxo-1H,2H-[1,2,4]triazolo[4,3-a]quinoxalin-4-yl]carbamoyl}propanamido)ethoxy]ethoxy}ethyl carbamate

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 50 ℃; for 18h;
DOI:10.1021/jm201722y

Reference yield:

: 153086-78-3
tert-butyl {2-[2-(2-aminoethoxy)ethoxy]ethyl}carbamate

: 1359959-28-6
tert-butyl N-2-{2-[2-(3-{[2-(4-methoxyphenyl)-1-oxo-1H,2H-[1,2,4]triazolo[4,3-a]quinoxalin-4-yl]carbamoyl}propanamido)ethoxy]ethoxy}ethyl carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: chloroform / 12 h / 0 - 20 °C

2: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 18 h / 50 °C

With 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU; In chloroform; N,N-dimethyl-formamide;
DOI:10.1021/jm201722y