N⁶-benzoyl-5'(S)-5'--2',3'-O-isopropylidene-5',5'-C,N-methylideneadenosine

Base Information

Chemical Name:N⁶-benzoyl-5'(S)-5'--2',3'-O-isopropylidene-5',5'-C,N-methylideneadenosine
CAS No.:107961-50-2
Molecular Formula:C₂₆H₃₀N₆O₆
Molecular Weight:522.561
Hs Code.:

N<sup>6</sup>-benzoyl-5'(S)-5'-<N-(tert-butyloxycarbonyl)amino>-2',3'-O-isopropylidene-5',5'-C,N-methylideneadenosine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N⁶-benzoyl-5'(S)-5'--2',3'-O-isopropylidene-5',5'-C,N-methylideneadenosine

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Technology Process of N⁶-benzoyl-5'(S)-5'--2',3'-O-isopropylidene-5',5'-C,N-methylideneadenosine

There total 5 articles about N⁶-benzoyl-5'(S)-5'--2',3'-O-isopropylidene-5',5'-C,N-methylideneadenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 107961-45-5
N⁶-benzoyl-5'(R)-C-<methyl>-2',3'-O-isopropylidene-5'-O-(p-toluenesulfonyl)adenosine

: 107961-50-2,107961-51-3
N⁶-benzoyl-5'(S)-5'--2',3'-O-isopropylidene-5',5'-C,N-methylideneadenosine

Guidance literature:: With potassium tert-butylate; In tert-butyl alcohol; at 20 ℃; for 1h;
DOI:10.1021/jm00388a024

Reference yield:

: 84757-69-7
N⁶-benzoyl-5'(R)-C-(nitromethyl)-2',3'-O-isopropylideneadenosine

: 107961-50-2,107961-51-3
N⁶-benzoyl-5'(S)-5'--2',3'-O-isopropylidene-5',5'-C,N-methylideneadenosine

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / PtO₂ / methanol / 16 h / 20 °C / 2585.7 Torr

2: CH₂Cl₂ / 1 h / 20 °C

3: 85 percent / pyridine / 28 h / 20 °C

4: 67 percent / t-BuOK / 2-methyl-propan-2-ol / 1 h / 20 °C

With pyridine; potassium tert-butylate; hydrogen; platinum(IV) oxide; In methanol; dichloromethane; tert-butyl alcohol;
DOI:10.1021/jm00388a024

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 107961-50-2,107961-51-3
N⁶-benzoyl-5'(S)-5'--2',3'-O-isopropylidene-5',5'-C,N-methylideneadenosine

Guidance literature:: Multi-step reaction with 3 steps

1: CH₂Cl₂ / 1 h / 20 °C

2: 85 percent / pyridine / 28 h / 20 °C

3: 67 percent / t-BuOK / 2-methyl-propan-2-ol / 1 h / 20 °C

With pyridine; potassium tert-butylate; In dichloromethane; tert-butyl alcohol;
DOI:10.1021/jm00388a024