C₅₄H₆₃N₃O₁₂

Base Information

Chemical Name:C₅₄H₆₃N₃O₁₂
CAS No.:1313731-14-4
Molecular Formula:C₅₄H₆₃N₃O₁₂
Molecular Weight:946.107
Hs Code.:

C<sub>54</sub>H<sub>63</sub>N<sub>3</sub>O<sub>12</sub>

Synonyms:

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Chemical Property of C₅₄H₆₃N₃O₁₂

Chemical Property:

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Technology Process of C₅₄H₆₃N₃O₁₂

There total 4 articles about C₅₄H₆₃N₃O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 112-35-6,95507-80-5
triethylene glucol monomethyl ether

: 1313731-14-4
C₅₄H₆₃N₃O₁₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydroxide / tetrahydrofuran / Inert atmosphere

2.1: sodium azide / water; acetone / Inert atmosphere

3.1: triphenylphosphine / tetrahydrofuran / Inert atmosphere

3.2: Inert atmosphere

4.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0 °C / Inert atmosphere

4.2: 0 - 20 °C / Inert atmosphere

5.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 40 h / 70 °C / Inert atmosphere

With dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; sodium azide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; acetone;
DOI:10.1021/jo201055t

Reference yield:

: 74654-07-2,80506-64-5,869718-87-6
2-[2-(2-methoxyethoxy)ethoxy]ethylamine

: 1313731-14-4
C₅₄H₆₃N₃O₁₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 40 h / 70 °C / Inert atmosphere

With dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo201055t

Reference yield:

: 62921-74-8,518012-62-9,58320-73-3
2-(2-(2-methoxyethoxy)ethoxy)ethyl p-toluenesulfonate

: 1313731-14-4
C₅₄H₆₃N₃O₁₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium azide / water; acetone / Inert atmosphere

2.1: triphenylphosphine / tetrahydrofuran / Inert atmosphere

2.2: Inert atmosphere

3.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0 °C / Inert atmosphere

3.2: 0 - 20 °C / Inert atmosphere

4.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 40 h / 70 °C / Inert atmosphere

With dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; sodium azide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; water; acetone;
DOI:10.1021/jo201055t