C₂₄H₄₂O₇SSi

Base Information

Chemical Name:C₂₄H₄₂O₇SSi
CAS No.:1431725-71-1
Molecular Formula:C₂₄H₄₂O₇SSi
Molecular Weight:502.745
Hs Code.:

C<sub>24</sub>H<sub>42</sub>O<sub>7</sub>SSi

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₄H₄₂O₇SSi

Chemical Property:

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Technology Process of C₂₄H₄₂O₇SSi

There total 7 articles about C₂₄H₄₂O₇SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1431725-92-6
C₁₈H₃₇IO₅Si

: 873-55-2
sodium benzenesulfonate

: 1431725-71-1
C₂₄H₄₂O₇SSi

Guidance literature:: In N,N-dimethyl-formamide; at 20 ℃; for 48h; Inert atmosphere;
DOI:10.1002/anie.201203406

Reference yield:

: 186641-79-2
(R)-4-((tert-Butyldiphenylsilyl)oxy)-3-methylbutanal

: 1431725-71-1
C₂₄H₄₂O₇SSi

Guidance literature:: Multi-step reaction with 8 steps

1.1: dichloromethane / 18 h / 55 °C

2.1: pyridinium p-toluenesulfonate / benzene / 48 h / Reflux

3.1: water; AD-mix-α; methanesulfonamide / tert-butyl alcohol / 36 h / 0 °C

4.1: 2,6-dimethylpyridine / dichloromethane / 0.08 h / -90 °C / Inert atmosphere

5.1: sodium iodide / 1,2-dimethoxyethane / 1 h / 20 °C / Inert atmosphere

5.2: 13 h / 20 °C / Inert atmosphere; Heating

6.1: H₃N*FH*3H₂O / methanol / 24 h / Inert atmosphere; Reflux

7.1: 1H-imidazole; iodine; triphenylphosphine / toluene / 0.5 h / Inert atmosphere

8.1: N,N-dimethyl-formamide / 48 h / 20 °C / Inert atmosphere

With 1H-imidazole; 2,6-dimethylpyridine; methanesulfonamide; AD-mix-α; H₃N*FH*3H₂O; water; iodine; pyridinium p-toluenesulfonate; triphenylphosphine; sodium iodide; In methanol; 1,2-dimethoxyethane; dichloromethane; N,N-dimethyl-formamide; toluene; tert-butyl alcohol; benzene; 1.1: |Wittig Olefination / 3.1: |Sharpless Dihydroxylation;
DOI:10.1002/anie.201203406

Reference yield:

: 1431725-69-7
C₃₂H₅₂O₅Si₂

: 1431725-71-1
C₂₄H₄₂O₇SSi

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium iodide / 1,2-dimethoxyethane / 1 h / 20 °C / Inert atmosphere

1.2: 13 h / 20 °C / Inert atmosphere; Heating

2.1: H₃N*FH*3H₂O / methanol / 24 h / Inert atmosphere; Reflux

3.1: 1H-imidazole; iodine; triphenylphosphine / toluene / 0.5 h / Inert atmosphere

4.1: N,N-dimethyl-formamide / 48 h / 20 °C / Inert atmosphere

With 1H-imidazole; H₃N*FH*3H₂O; iodine; triphenylphosphine; sodium iodide; In methanol; 1,2-dimethoxyethane; N,N-dimethyl-formamide; toluene;
DOI:10.1002/anie.201203406