Technology Process of (13)C18H12O3
There total 6 articles about (13)C18H12O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: aluminum (III) chloride / 1,1,2,2-tetrachloroethane
2.1: hydrazine hydrate / diethylene glycol / 0.5 h / 20 °C
2.2: 120 - 215 °C
3.1: methanesulfonic acid / 0.5 h / 90 °C / Inert atmosphere
4.1: diethylsulfone; potassium tert-butylate / N,N-dimethyl acetamide / 150 °C / Inert atmosphere
5.1: aluminum (III) chloride
With
aluminum (III) chloride; methanesulfonic acid; diethylsulfone; potassium tert-butylate; hydrazine hydrate;
In
N,N-dimethyl acetamide; 1,1,2,2-tetrachloroethane; diethylene glycol;
2.1: Wolff-Kishner reduction / 2.2: Wolff-Kishner reduction / 5.1: Friedel-Crafts condensation;
DOI:10.1039/c0ob01107j
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrazine hydrate / diethylene glycol / 0.5 h / 20 °C
1.2: 120 - 215 °C
2.1: methanesulfonic acid / 0.5 h / 90 °C / Inert atmosphere
3.1: diethylsulfone; potassium tert-butylate / N,N-dimethyl acetamide / 150 °C / Inert atmosphere
4.1: aluminum (III) chloride
With
aluminum (III) chloride; methanesulfonic acid; diethylsulfone; potassium tert-butylate; hydrazine hydrate;
In
N,N-dimethyl acetamide; diethylene glycol;
1.1: Wolff-Kishner reduction / 1.2: Wolff-Kishner reduction / 4.1: Friedel-Crafts condensation;
DOI:10.1039/c0ob01107j
- Guidance literature:
-
Multi-step reaction with 3 steps
1: methanesulfonic acid / 0.5 h / 90 °C / Inert atmosphere
2: diethylsulfone; potassium tert-butylate / N,N-dimethyl acetamide / 150 °C / Inert atmosphere
3: aluminum (III) chloride
With
aluminum (III) chloride; methanesulfonic acid; diethylsulfone; potassium tert-butylate;
In
N,N-dimethyl acetamide;
3: Friedel-Crafts condensation;
DOI:10.1039/c0ob01107j