3-(4-methoxybenzyloxy)propyltriphenylphosphonium bromide

Base Information

• Chemical Name: 3-(4-methoxybenzyloxy)propyltriphenylphosphonium bromide
• CAS No.: 1042909-01-2
• Molecular Formula: Br*C₂₉H₃₀O₂P
• Molecular Weight: 521.434
• Mol file: 1042909-01-2.mol

Synonyms:

Chemical Property of 3-(4-methoxybenzyloxy)propyltriphenylphosphonium bromide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-(4-methoxybenzyloxy)propyltriphenylphosphonium bromide

There total 1 articles about 3-(4-methoxybenzyloxy)propyltriphenylphosphonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

triphenylphosphine (603-35-0) + 1-[(3-bromopropoxy)methyl]-4-methoxybenzene (147193-45-1) → 3-(4-methoxybenzyloxy)propyltriphenylphosphonium bromide (1042909-01-2)

Guidance literature:

Heating;

DOI:10.1021/jo800514k

Reference yield:

3-(4-methoxybenzyloxy)propyltriphenylphosphonium bromide (1042909-01-2) + 5-(trimethylsilyl)pent-4-ynal (68654-85-3) → (Z)-{8-[(4-methoxybenzyl)oxy]oct-5-en-1-yn-1-yl}trimethylsilane

Guidance literature:

3-(4-methoxybenzyloxy)propyltriphenylphosphonium bromide; With potassium hexamethylsilazane; In tetrahydrofuran; toluene; at -78 ℃; for 0.333333h;

5-(trimethylsilyl)pent-4-ynal; In tetrahydrofuran; toluene; at -78 ℃; for 0.5h; stereoselective reaction;

DOI:10.1002/ejoc.201701562

upstream raw materials:

triphenylphosphine

1-[(3-bromopropoxy)methyl]-4-methoxybenzene