Technology Process of ethyl pyruvate 2-
There total 7 articles about ethyl pyruvate 2- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 41.7 percent / K2CO3, CuBr / nitrobenzene / 3.5 h / 180 - 190 °C
2: 91.5 percent / KOH / ethane-1,2-diol / 2 h / 150 - 160 °C
3: 78.9 percent / CF3CO2H / benzene / 5 h / Ambient temperature
4: 85 percent / 14percent NaOH aq., NaOCl (containing 10.2percent active chlorine) / ethanol / 1 h / Ambient temperature
5: ethanol / Heating
With
potassium hydroxide; sodium hydroxide; sodium hypochlorite; potassium carbonate; trifluoroacetic acid; copper(I) bromide;
In
ethanol; ethylene glycol; nitrobenzene; benzene;
DOI:10.1248/cpb.31.423
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 85 percent / 14percent NaOH aq., NaOCl (containing 10.2percent active chlorine) / ethanol / 1 h / Ambient temperature
2: ethanol / Heating
With
sodium hydroxide; sodium hypochlorite;
In
ethanol;
DOI:10.1248/cpb.31.423
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 78.9 percent / CF3CO2H / benzene / 5 h / Ambient temperature
2: 85 percent / 14percent NaOH aq., NaOCl (containing 10.2percent active chlorine) / ethanol / 1 h / Ambient temperature
3: ethanol / Heating
With
sodium hydroxide; sodium hypochlorite; trifluoroacetic acid;
In
ethanol; benzene;
DOI:10.1248/cpb.31.423