C₁₈H₁₃Br₃N₂O₃

Base Information

Chemical Name:C₁₈H₁₃Br₃N₂O₃
CAS No.:1422285-77-5
Molecular Formula:C₁₈H₁₃Br₃N₂O₃
Molecular Weight:545.025
Hs Code.:

C<sub>18</sub>H<sub>13</sub>Br<sub>3</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:

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Chemical Property of C₁₈H₁₃Br₃N₂O₃

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Technology Process of C₁₈H₁₃Br₃N₂O₃

There total 5 articles about C₁₈H₁₃Br₃N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1422285-76-4
C₁₈H₁₄Br₃NO₅

: 1422285-77-5
C₁₈H₁₃Br₃N₂O₃

Guidance literature:: With ammonium acetate; In ethanol;
DOI:10.1016/j.bmcl.2012.12.033

Reference yield:

: 99-93-4
4-Hydroxyacetophenone

: 1422285-77-5
C₁₈H₁₃Br₃N₂O₃

Guidance literature:: Multi-step reaction with 6 steps

1: bromine / acetic acid / 2 h / 20 °C

2: bromine / chloroform / 2 h / 20 °C

3: chloroform / 18 h / 20 °C

4: hydrogen bromide / methanol / 48 h

5: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; 4-methyl-morpholine / N,N-dimethyl-formamide / 2 h / 20 °C

6: ammonium acetate / ethanol

With 4-methyl-morpholine; ammonium acetate; hydrogen bromide; bromine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; In methanol; ethanol; chloroform; acetic acid; N,N-dimethyl-formamide; 2: |Delepine Amine Synthesis;
DOI:10.1016/j.bmcl.2012.12.033

Reference yield:

: 2887-72-1
1-(3,5-dibromo-4-hydroxyphenyl)ethan-1-one

: 1422285-77-5
C₁₈H₁₃Br₃N₂O₃

Guidance literature:: Multi-step reaction with 5 steps

1: bromine / chloroform / 2 h / 20 °C

2: chloroform / 18 h / 20 °C

3: hydrogen bromide / methanol / 48 h

4: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; 4-methyl-morpholine / N,N-dimethyl-formamide / 2 h / 20 °C

5: ammonium acetate / ethanol

With 4-methyl-morpholine; ammonium acetate; hydrogen bromide; bromine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; In methanol; ethanol; chloroform; N,N-dimethyl-formamide; 1: |Delepine Amine Synthesis;
DOI:10.1016/j.bmcl.2012.12.033