(2R,3S,4S)-2-hydroxy-3,4-epoxy-3-methyl-4-phenylbutanoic acid methylester

Base Information

Chemical Name:(2R,3S,4S)-2-hydroxy-3,4-epoxy-3-methyl-4-phenylbutanoic acid methylester
CAS No.:140924-06-7
Molecular Formula:C₁₂H₁₄O₄
Molecular Weight:222.241
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3S,4S)-2-hydroxy-3,4-epoxy-3-methyl-4-phenylbutanoic acid methylester

Chemical Property:

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Technology Process of (2R,3S,4S)-2-hydroxy-3,4-epoxy-3-methyl-4-phenylbutanoic acid methylester

There total 2 articles about (2R,3S,4S)-2-hydroxy-3,4-epoxy-3-methyl-4-phenylbutanoic acid methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 140632-59-3
(E)-(R)-2-Hydroxy-3-methyl-4-phenyl-but-3-enoic acid

: 140924-06-7
(2R,3S,4S)-2-hydroxy-3,4-epoxy-3-methyl-4-phenylbutanoic acid methylester

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / HCl gas

2: MCPBA / hexane; diethyl ether / 72 h / Ambient temperature

With hydrogenchloride; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; hexane;
DOI:10.1016/S0040-4020(01)86507-8

Reference yield:

: 140479-56-7
(E)-(R)-2-Hydroxy-3-methyl-4-phenyl-but-3-enoic acid methyl ester

: 140479-59-0
(2R,3R,4R)-2-hydroxy-3,4-epoxy-3-methyl-4-phenylbutanoic acid methylester

: 140924-06-7
(2R,3S,4S)-2-hydroxy-3,4-epoxy-3-methyl-4-phenylbutanoic acid methylester

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In diethyl ether; hexane; for 72h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;
DOI:10.1016/S0040-4020(01)86507-8