CpTi(3,5-diphenylpyrazolato)Cl₂

Base Information

• Chemical Name: CpTi(3,5-diphenylpyrazolato)Cl₂
• CAS No.: 1152411-52-3
• Molecular Formula: C₂₀H₁₆Cl₂N₂Ti
• Molecular Weight: 403.146
• Mol file: 1152411-52-3.mol

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Chemical Property of CpTi(3,5-diphenylpyrazolato)Cl₂

Chemical Property:

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Technology Process of CpTi(3,5-diphenylpyrazolato)Cl₂

There total 1 articles about CpTi(3,5-diphenylpyrazolato)Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

cyclopentadienyl titanium(IV) trichloride (1270-98-0) + Li[3,5-dimethylpyrazolate] → CpTi(3,5-diphenylpyrazolato)Cl2 (1152411-52-3)

Guidance literature:

In diethyl ether; (N2) to soln. Ti complex in Et2O at -20°C Li salt ligand was added (1:1), stirred at 25°C for 16 h; CH2Cl2 was added, soln. was filtered through Celite and evapd. in vacuo,residue was dissolved in CH2Cl2 and layered with n-hexane (-20°C ); elem. anal.;

DOI:10.1021/ic9004246

upstream raw materials:

cyclopentadienyl titanium(IV) trichloride