Technology Process of C25H35NO4*ClH
There total 6 articles about C25H35NO4*ClH which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hydrogenchloride / water / 12 h / 20 °C
2: tetrahydrofuran / 12 h / 20 °C
3: palladium diacetate; ammonium formate / methanol / 0.5 h / Reflux
4: ethanol / 24 h / Reflux
5: hydrogenchloride / diethyl ether
With
hydrogenchloride; ammonium formate; palladium diacetate;
In
tetrahydrofuran; methanol; diethyl ether; ethanol; water;
DOI:10.1016/j.bmcl.2013.03.092
- Guidance literature:
-
Multi-step reaction with 6 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 24 h / Reflux
2: hydrogenchloride / water / 12 h / 20 °C
3: tetrahydrofuran / 12 h / 20 °C
4: palladium diacetate; ammonium formate / methanol / 0.5 h / Reflux
5: ethanol / 24 h / Reflux
6: hydrogenchloride / diethyl ether
With
hydrogenchloride; lithium aluminium tetrahydride; ammonium formate; palladium diacetate;
In
tetrahydrofuran; methanol; diethyl ether; ethanol; water;
DOI:10.1016/j.bmcl.2013.03.092
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetrahydrofuran / 12 h / 20 °C
2: palladium diacetate; ammonium formate / methanol / 0.5 h / Reflux
3: ethanol / 24 h / Reflux
4: hydrogenchloride / diethyl ether
With
hydrogenchloride; ammonium formate; palladium diacetate;
In
tetrahydrofuran; methanol; diethyl ether; ethanol;
DOI:10.1016/j.bmcl.2013.03.092
