C₁₁H₁₄IN

Base Information

Chemical Name:C₁₁H₁₄IN
CAS No.:1416476-20-4
Molecular Formula:C₁₁H₁₄IN
Molecular Weight:287.143
Hs Code.:

Synonyms:

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Chemical Property of C₁₁H₁₄IN

Chemical Property:

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Technology Process of C₁₁H₁₄IN

There total 4 articles about C₁₁H₁₄IN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1530-32-1
ethyltriphenylphosphonium bromide

: 385416-65-9
2-iodo-5-(N,N-dimethylamino)benzaldehyde

: 1416476-20-4
C₁₁H₁₄IN

: 1416476-24-8
C₁₁H₁₄IN

Guidance literature:: ethyltriphenylphosphonium bromide; With potassium 2-methylbutan-2-olate; In tetrahydrofuran; for 0.166667h; Inert atmosphere;

2-iodo-5-(N,N-dimethylamino)benzaldehyde; In tetrahydrofuran; at 20 ℃; for 0.5h; Overall yield = 99 %; Cooling with ice; Inert atmosphere;
DOI:10.1039/c2dt32422a

Reference yield:

: 99-64-9
3-(dimethylamino)benzoic acid

: 1416476-20-4
C₁₁H₁₄IN

: 1416476-24-8
C₁₁H₁₄IN

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium tetrahydroborate / tetrahydrofuran / 0.25 h / Inert atmosphere; Cooling

1.2: 4.5 h / 20 - 70 °C / Inert atmosphere

2.1: sodium hydrogencarbonate; iodine / dichloromethane; water / 20 °C

3.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 0.42 h / -80 - -65 °C / Inert atmosphere

3.2: 0.75 h / -65 - 20 °C / Inert atmosphere

4.1: potassium 2-methylbutan-2-olate / tetrahydrofuran / 0.17 h / Inert atmosphere

4.2: 0.5 h / 20 °C / Cooling with ice; Inert atmosphere

With sodium tetrahydroborate; oxalyl dichloride; iodine; potassium 2-methylbutan-2-olate; sodium hydrogencarbonate; dimethyl sulfoxide; In tetrahydrofuran; dichloromethane; water;
DOI:10.1039/c2dt32422a

Reference yield:

: 23501-93-1
3-dimethylaminobenzyl alcohol

: 1416476-20-4
C₁₁H₁₄IN

: 1416476-24-8
C₁₁H₁₄IN

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydrogencarbonate; iodine / dichloromethane; water / 20 °C

2.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 0.42 h / -80 - -65 °C / Inert atmosphere

2.2: 0.75 h / -65 - 20 °C / Inert atmosphere

3.1: potassium 2-methylbutan-2-olate / tetrahydrofuran / 0.17 h / Inert atmosphere

3.2: 0.5 h / 20 °C / Cooling with ice; Inert atmosphere

With oxalyl dichloride; iodine; potassium 2-methylbutan-2-olate; sodium hydrogencarbonate; dimethyl sulfoxide; In tetrahydrofuran; dichloromethane; water;
DOI:10.1039/c2dt32422a