C₃₀H₃₁F₉N₆O₂

Base Information

Chemical Name:C₃₀H₃₁F₉N₆O₂
CAS No.:874502-03-1
Molecular Formula:C₃₀H₃₁F₉N₆O₂
Molecular Weight:678.601
Hs Code.:

C<sub>30</sub>H<sub>31</sub>F<sub>9</sub>N<sub>6</sub>O<sub>2</sub>

Synonyms:

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Chemical Property of C₃₀H₃₁F₉N₆O₂

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Technology Process of C₃₀H₃₁F₉N₆O₂

There total 10 articles about C₃₀H₃₁F₉N₆O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 874501-94-7
C₂₆H₂₅F₉N₆O₂

: 874502-03-1
C₃₀H₃₁F₉N₆O₂

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; acetone; at 20 ℃;
DOI:10.1016/j.bmcl.2012.04.042

Reference yield:

: (3R)-[3-(4-trifluoromethylphenylamino)pentanoyl]carbamic acid benzyl ester

: 874502-03-1
C₃₀H₃₁F₉N₆O₂

Guidance literature:: Multi-step reaction with 7 steps

1: sodium tetrahydroborate; magnesium chloride / ethanol; water

2: pyridine / 0 - 20 °C

3: palladium 10% on activated carbon; hydrogen / ethyl acetate / 760.05 Torr

4: sodium tris(acetoxy)borohydride; acetic acid / 1,1-dichloroethane / 20 °C

5: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C

6: sodium azide; triethylamine / toluene / 110 °C

7: potassium carbonate / N,N-dimethyl-formamide; acetone / 20 °C

With pyridine; sodium tetrahydroborate; sodium azide; sodium tris(acetoxy)borohydride; palladium 10% on activated carbon; hydrogen; potassium carbonate; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; magnesium chloride; In tetrahydrofuran; 1,1-dichloroethane; ethanol; water; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1016/j.bmcl.2012.04.042

Reference yield:

: 474645-96-0
(2R,4S)-(2-ethyl-6-trifluoromethyl-1,2,3,4-tetrahydroquinolin-4-yl)carbamic acid benzyl ester

: 874502-03-1
C₃₀H₃₁F₉N₆O₂

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine / 0 - 20 °C

2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 760.05 Torr

3: sodium tris(acetoxy)borohydride; acetic acid / 1,1-dichloroethane / 20 °C

4: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C

5: sodium azide; triethylamine / toluene / 110 °C

6: potassium carbonate / N,N-dimethyl-formamide; acetone / 20 °C

With pyridine; sodium azide; sodium tris(acetoxy)borohydride; palladium 10% on activated carbon; hydrogen; potassium carbonate; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 1,1-dichloroethane; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1016/j.bmcl.2012.04.042