methyl(3-diphenylphosphanyl)-2-thionaphtholato[P,S](trimethylphosphine)nickel

Base Information

Chemical Name:methyl(3-diphenylphosphanyl)-2-thionaphtholato[P,S](trimethylphosphine)nickel
CAS No.:1161924-35-1
Molecular Formula:C₂₆H₂₈NiP₂S
Molecular Weight:493.212
Hs Code.:

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Chemical Property of methyl(3-diphenylphosphanyl)-2-thionaphtholato[P,S](trimethylphosphine)nickel

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Technology Process of methyl(3-diphenylphosphanyl)-2-thionaphtholato[P,S](trimethylphosphine)nickel

There total 2 articles about methyl(3-diphenylphosphanyl)-2-thionaphtholato[P,S](trimethylphosphine)nickel which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: [Ni(OMe)(Me)(trimethylphosphine)]

: 1161924-37-3
(3-diphenylphosphanyl)-2-thionaphthol

: 1161924-35-1
methyl(3-diphenylphosphanyl)-2-thionaphtholato[P,S](trimethylphosphine)nickel

Guidance literature:: In tetrahydrofuran; byproducts: trimetylphosphine, CH4; combining of soln. of Ni(OMe)Me(PMe3) in THF with (3-diphenylphosphanyl)-2-thionaphthol for 10 min; removal of volatiles in vac., extn. with pentane; crystn. at room temp.,elem. anal.;
DOI:10.1016/j.jorganchem.2009.01.023

Reference yield:

: NiMe₂(PMe₃)3

: 1161924-37-3
(3-diphenylphosphanyl)-2-thionaphthol

: 1161924-35-1
methyl(3-diphenylphosphanyl)-2-thionaphtholato[P,S](trimethylphosphine)nickel

Guidance literature:: In tetrahydrofuran; byproducts: trimetylphosphine, CH4; combining of soln. of NiMe2(PMe3) in THF with (3-diphenylphosphanyl)-2-thionaphthol;
DOI:10.1016/j.jorganchem.2009.01.023