iso-propyl 3,4,6-tri-O-benzyl-2-deoxy-2-(2,4-dinitrophenylamino)-α-D-glucopyranosyl-(1->4)-(methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosyluronate)

Base Information

Chemical Name:iso-propyl 3,4,6-tri-O-benzyl-2-deoxy-2-(2,4-dinitrophenylamino)-α-D-glucopyranosyl-(1->4)-(methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosyluronate)
CAS No.:1203584-63-7
Molecular Formula:C₅₅H₆₃N₃O₁₆
Molecular Weight:1022.12
Hs Code.:

iso-propyl 3,4,6-tri-O-benzyl-2-deoxy-2-(2,4-dinitrophenylamino)-α-D-glucopyranosyl-(1->4)-(methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosyluronate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of iso-propyl 3,4,6-tri-O-benzyl-2-deoxy-2-(2,4-dinitrophenylamino)-α-D-glucopyranosyl-(1->4)-(methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosyluronate)

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Technology Process of iso-propyl 3,4,6-tri-O-benzyl-2-deoxy-2-(2,4-dinitrophenylamino)-α-D-glucopyranosyl-(1->4)-(methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosyluronate)

There total 4 articles about iso-propyl 3,4,6-tri-O-benzyl-2-deoxy-2-(2,4-dinitrophenylamino)-α-D-glucopyranosyl-(1->4)-(methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosyluronate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1203584-60-4
iso-propyl (methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosyluronate)

: 3,4,6-tri-O-benzyl-2-deoxy-2-(2,4-dinitrophenylamino)-D-glucopyranosyl trichloroacetimidate

: iso-propyl 3,4,6-tri-O-benzyl-2-deoxy-2-(2,4-dinitrophenylamino)-β-D-glucopyranosyl-(1->4)-(methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosyluronate)

: 1203584-63-7
iso-propyl 3,4,6-tri-O-benzyl-2-deoxy-2-(2,4-dinitrophenylamino)-α-D-glucopyranosyl-(1->4)-(methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosyluronate)

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In diethyl ether; dichloromethane; at -29 - -10 ℃; for 0.75h; optical yield given as %de; Molecular sieve; Inert atmosphere;
DOI:10.1080/07328300903105108

Reference yield:

: 1203584-60-4
iso-propyl (methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosyluronate)

: 3,4,6-tri-O-benzyl-2-deoxy-2-(2,4-dinitrophenylamino)-D-glucopyranosyl dibutyl phosphate

: iso-propyl 3,4,6-tri-O-benzyl-2-deoxy-2-(2,4-dinitrophenylamino)-β-D-glucopyranosyl-(1->4)-(methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosyluronate)

: 1203584-63-7
iso-propyl 3,4,6-tri-O-benzyl-2-deoxy-2-(2,4-dinitrophenylamino)-α-D-glucopyranosyl-(1->4)-(methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosyluronate)

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 - -50 ℃; for 0.5h; optical yield given as %de; Molecular sieve; Inert atmosphere;
DOI:10.1080/07328300903105108

Reference yield:

: 1203584-60-4
iso-propyl (methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosyluronate)

: 3,4,6-tri-O-benzyl-2-deoxy-2-(2,4-dinitrophenylamino)-D-glucopyranosyl N-(phenyl)trifluoroacetimidate

: iso-propyl 3,4,6-tri-O-benzyl-2-deoxy-2-(2,4-dinitrophenylamino)-β-D-glucopyranosyl-(1->4)-(methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosyluronate)

: 1203584-63-7
iso-propyl 3,4,6-tri-O-benzyl-2-deoxy-2-(2,4-dinitrophenylamino)-α-D-glucopyranosyl-(1->4)-(methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosyluronate)

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -30 - -5 ℃; for 0.75h; optical yield given as %de; Molecular sieve; Inert atmosphere;
DOI:10.1080/07328300903105108